C₂₂H₁₉Cl₂N₃O₅S

Base Information

• Chemical Name: C₂₂H₁₉Cl₂N₃O₅S
• CAS No.: 1416363-90-0
• Molecular Formula: C₂₂H₁₉Cl₂N₃O₅S
• Molecular Weight: 508.382
• Mol file: 1416363-90-0.mol

Synonyms:

Chemical Property of C₂₂H₁₉Cl₂N₃O₅S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₁₉Cl₂N₃O₅S

There total 3 articles about C₂₂H₁₉Cl₂N₃O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C8H5Cl2NO4 (75263-82-0) → C22H19Cl2N3O5S (1416363-90-0)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydrogencarbonate / acetone / 2 h / 80 °C

2: ammonium chloride; iron / acetone; water / 12 h / 80 °C

3: sodium hydrogencarbonate / acetone / 0.67 h / 0 - 20 °C

With iron; sodium hydrogencarbonate; ammonium chloride; In water; acetone;

DOI:10.1016/j.ejmech.2012.03.032

Reference yield:

(4-chloro-2-nitro-phenoxy)-acetic acid (21086-49-7) → C22H19Cl2N3O5S (1416363-90-0)

Guidance literature:

Multi-step reaction with 4 steps

1: thionyl chloride / 80 °C

2: sodium hydrogencarbonate / acetone / 2 h / 80 °C

3: ammonium chloride; iron / acetone; water / 12 h / 80 °C

4: sodium hydrogencarbonate / acetone / 0.67 h / 0 - 20 °C

With thionyl chloride; iron; sodium hydrogencarbonate; ammonium chloride; In water; acetone;

DOI:10.1016/j.ejmech.2012.03.032

Reference yield:

N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide (1341199-23-2) → C22H19Cl2N3O5S (1416363-90-0)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonium chloride; iron / acetone; water / 12 h / 80 °C

2: sodium hydrogencarbonate / acetone / 0.67 h / 0 - 20 °C

With iron; sodium hydrogencarbonate; ammonium chloride; In water; acetone;

DOI:10.1016/j.ejmech.2012.03.032

upstream raw materials:

N-[4-(aminosulfonyl)-2-methylphenyl]-2-(4-chloro-2-nitrophenoxy)acetamide

C₈H₅Cl₂NO₄

(4-chloro-2-nitro-phenoxy)-acetic acid