N-(benzyloxycarbonyl) [4,6-di-O-acetyl-2-azido-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-O-(2,5-difluorobenzoyl)-β-D-galactopyranosyl)-(1->3)-α-D-galactopyranosyl]-L-serine t-butyl ester

Base Information

• Chemical Name: N-(benzyloxycarbonyl) [4,6-di-O-acetyl-2-azido-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-O-(2,5-difluorobenzoyl)-β-D-galactopyranosyl)-(1->3)-α-D-galactopyranosyl]-L-serine t-butyl ester
• CAS No.: 1045786-04-6
• Molecular Formula: C₄₄H₅₂F₂N₄O₂₀
• Molecular Weight: 994.908

Synonyms:

Chemical Property of N-(benzyloxycarbonyl) [4,6-di-O-acetyl-2-azido-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-O-(2,5-difluorobenzoyl)-β-D-galactopyranosyl)-(1->3)-α-D-galactopyranosyl]-L-serine t-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of N-(benzyloxycarbonyl) [4,6-di-O-acetyl-2-azido-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-O-(2,5-difluorobenzoyl)-β-D-galactopyranosyl)-(1->3)-α-D-galactopyranosyl]-L-serine t-butyl ester

There total 1 articles about N-(benzyloxycarbonyl) [4,6-di-O-acetyl-2-azido-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-O-(2,5-difluorobenzoyl)-β-D-galactopyranosyl)-(1->3)-α-D-galactopyranosyl]-L-serine t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C40H48F2N4O18 + acetic anhydride (108-24-7) → N-(benzyloxycarbonyl) [4,6-di-O-acetyl-2-azido-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-O-(2,5-difluorobenzoyl)-β-D-galactopyranosyl)-(1->3)-α-D-galactopyranosyl]-L-serine t-butyl ester (1045786-04-6)

Guidance literature:

With pyridine; dmap; for 12h;

DOI:10.1016/j.carres.2008.05.002

Reference yield: 67.0%

N-(benzyloxycarbonyl) [4,6-di-O-acetyl-2-azido-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-O-(2,5-difluorobenzoyl)-β-D-galactopyranosyl)-(1->3)-α-D-galactopyranosyl]-L-serine t-butyl ester (1045786-04-6) + tiolacetic acid (507-09-5) → N-(benzyloxycarbonyl) [2-acetamido-4,6-di-O-acetyl-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-O-(2,5-difluorobenzoyl)-β-D-galactopyranosyl)-(1->3)-α-D-galactopyranosyl]-L-serine t-butyl ester (1045786-06-8)

Guidance literature:

With pyridine; for 18h;

DOI:10.1016/j.carres.2008.05.002

upstream raw materials:

acetic anhydride

Downstream raw materials:

N-(benzyloxycarbonyl) [2-acetamido-4,6-di-O-acetyl-2-deoxy-3-O-(3,4,6-tri-O-acetyl-2-O-(2,5-difluorobenzoyl)-β-D-galactopyranosyl)-(1->3)-α-D-galactopyranosyl]-L-serine t-butyl ester

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