1,3,2-Diazaborolidine, 1-methyl-2-phenyl-

Base Information

• Chemical Name: 1,3,2-Diazaborolidine, 1-methyl-2-phenyl-
• CAS No.: 6076-64-8
• Molecular Formula: C9H13 B N2
• Molecular Weight: 160.027
• DSSTox Substance ID: DTXSID10209582
• Wikidata: Q83083923

Synonyms:1,3,2-Diazaborolidine, 1-methyl-2-phenyl-;6076-64-8;1,3,2-Diazaborolidine,1-methyl-2-phenyl-;DTXSID10209582

Chemical Property of 1,3,2-Diazaborolidine, 1-methyl-2-phenyl-

Chemical Property:

• Vapor Pressure: 0.0692mmHg at 25°C
• Boiling Point: 229.5°C at 760 mmHg
• Flash Point: 92.6°C
• Density: 1.01g/cm³
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 1
• Exact Mass: 160.1171786
• Heavy Atom Count: 12
• Complexity: 146

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: B1(NCCN1C)C2=CC=CC=C2

Technology Process of 1,3,2-Diazaborolidine, 1-methyl-2-phenyl-

There total 2 articles about 1,3,2-Diazaborolidine, 1-methyl-2-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

Bis-(dimethylamino)-phenylboran (1201-45-2) + N-methyl-ethane-1,2-diamine (109-81-9) → 2-methyl-1-phenyl-1,3,2-diazaborolane (6076-64-8) + dimethyl amine (124-40-3)

Guidance literature:

transamination, boiling the educts in inert atmosphere, distn. of dimethylamine during reaction; distn.;

DOI:10.1021/ic50039a006

Reference yield:

→ 2-methyl-1-phenyl-1,3,2-diazaborolane (6076-64-8)

Guidance literature:

PhB(N(CH3)2)2, H2N-CH2-CH2-NH(CH3);

DOI:10.1021/ic50039a006

upstream raw materials:

Bis-(dimethylamino)-phenylboran

N-methyl-ethane-1,2-diamine

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