2--(2-2H)-3-methylbutyronitrile

Base Information

Chemical Name:2--(2-2H)-3-methylbutyronitrile
CAS No.:139512-46-2
Molecular Formula:C₁₈H₁₈N₂
Molecular Weight:263.346
Hs Code.:

2-<N-(diphenylmethylene)amino>-(2-2H)-3-methylbutyronitrile

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--(2-2H)-3-methylbutyronitrile

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 2--(2-2H)-3-methylbutyronitrile

There total 1 articles about 2--(2-2H)-3-methylbutyronitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70591-20-7
N-(diphenylmethylene)aminoacetonitrile

: 75-26-3
isopropyl bromide

: 139512-46-2
2--(2-2H)-3-methylbutyronitrile

Guidance literature:: With deuteriated sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; Yield given. Multistep reaction; 1) toluene, 0 deg C, 2) toluene, RT, overnight;
DOI:10.1016/S0040-4020(01)80725-0

Reference yield:

: 139512-46-2
2--(2-2H)-3-methylbutyronitrile

: C₇H₈O₃S*C₅H₁₀⁽²⁾HNO₂

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 1N HCl, 2) conc. HCl / 1) Et₂O, 12h, 2) 12h, reflux

2: tetrahydrofuran; H₂O

With hydrogenchloride; In tetrahydrofuran; water;
DOI:10.1016/S0040-4020(01)80725-0

Reference yield:

: 139512-46-2
2--(2-2H)-3-methylbutyronitrile

: D/L-(2-2H)-valine benzhydryl ester tosyl ammonium salt

Guidance literature:: Multi-step reaction with 3 steps

1: 1) 1N HCl, 2) conc. HCl / 1) Et₂O, 12h, 2) 12h, reflux

2: tetrahydrofuran; H₂O

3: acetonitrile

With hydrogenchloride; In tetrahydrofuran; water; acetonitrile;
DOI:10.1016/S0040-4020(01)80725-0