{RuCl(C₆H₅CN)5}⁽¹⁺⁾*BF₄^(1-)={RuCl(C₆H₅CN)5}BF₄

Base Information

Chemical Name:{RuCl(C₆H₅CN)5}⁽¹⁺⁾*BF₄^(1-)={RuCl(C₆H₅CN)5}BF₄
CAS No.:137355-22-7
Molecular Formula:BF₄*C₃₅H₂₅ClN₅Ru
Molecular Weight:738.945
Hs Code.:

{RuCl(C<sub>6</sub>H<sub>5</sub>CN)5}<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>={RuCl(C<sub>6</sub>H<sub>5</sub>CN)5}BF<sub>4</sub>

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Chemical Property of {RuCl(C₆H₅CN)5}⁽¹⁺⁾*BF₄^(1-)={RuCl(C₆H₅CN)5}BF₄

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Technology Process of {RuCl(C₆H₅CN)5}⁽¹⁺⁾*BF₄^(1-)={RuCl(C₆H₅CN)5}BF₄

There total 1 articles about {RuCl(C₆H₅CN)5}⁽¹⁺⁾*BF₄^(1-)={RuCl(C₆H₅CN)5}BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 14104-20-2
silver tetrafluoroborate

: 21503-87-7,51014-03-0
trans-{RuCl₂(C₆H₅CN)4}

: 100-47-0
benzonitrile

: 137355-22-7
{RuCl(C₆H₅CN)5}⁽¹⁺⁾*BF₄^(1-)={RuCl(C₆H₅CN)5}BF₄

Guidance literature:: In benzonitrile; the dichloro-complex was treated with AgBF4 (slight excess) in PhCN at 100 °C for 2 h; filtered through Celite;; after filtration through celite, the prod. was pptd. by addn. of diethyl ether/pentane 50:50 and recrystd. from benzonitrile-CH2Cl2(5:95) and diethyl ether; elem.anal.;;
DOI:10.1039/DT9910002401

Reference yield: 80.0%

: 137355-22-7
{RuCl(C₆H₅CN)5}⁽¹⁺⁾*BF₄^(1-)={RuCl(C₆H₅CN)5}BF₄

: 1493-13-6
trifluorormethanesulfonic acid

: 100-47-0
benzonitrile

: {Ru(C₆H₅CN)6}⁽²⁺⁾*2{CF₃SO₃}^(1-)={Ru(C₆H₅CN)6}{CF₃SO₃}2

Guidance literature:: In diethyl ether; benzonitrile; the monochlorocomplex was heated in triflic acid under strictly dry, anaerobic conditions at 100 °C for 1.5 h; after cooling, the soln. was dild. with diethyl ether and PhCN was added; the mixt. was added to water and the organic phase separated;; the organic phase was washed with water, dried over anhydrous Na2SO4, and concd.; the prod. was finally pptd. by addn. of pentane; elem.anal.;
DOI:10.1039/DT9910002401