[N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiMe

Base Information

Chemical Name:[N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiMe
CAS No.:1353054-93-9
Molecular Formula:C₃₁H₃₅NNiP₂
Molecular Weight:542.263
Hs Code.:

[N(o-C<sub>6</sub>H<sub>4</sub>PPh<sub>2</sub>)(o-C<sub>6</sub>H<sub>4</sub>P(i)Pr<sub>2</sub>)]NiMe

Synonyms:

Suppliers and Price of [N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiMe

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiMe

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiMe

There total 1 articles about [N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1332655-38-5
[N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiCl

: 676-58-4
methylmagnesium chloride

: 1353054-93-9
[N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiMe

Guidance literature:: In tetrahydrofuran; (N2); CH3MgCl in THF added dropwise to a soln. of Ni complex at -35°C, stirred at room temp. for 2 h; evapd. (vac.), triturated with pentane, C6H6 added, filtered, washed (C6H6), the combined filtrate evapd. (vac.); elem. anal.;
DOI:10.1021/om201041z

Reference yield: 92.0%

: 201230-82-2
carbon monoxide

: 1353054-93-9
[N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiMe

: 1353054-94-0
[N(o-C₆H₄PPh₂)(o-C₆H₄P(i)Pr₂)]NiC(O)Me

Guidance literature:: In benzene; (N2); a soln. of Ni complex degassed, CO (1 atm) introduced at room temp., stirred at room temp.; evapd. (vac.), triturated with pentane, dried (vac.); elem. anal.;
DOI:10.1021/om201041z