ethoxycarbonylmethyl 2-methyl-2-(p-tolylsulfonyl)propanedithioate

Base Information

Chemical Name:ethoxycarbonylmethyl 2-methyl-2-(p-tolylsulfonyl)propanedithioate
CAS No.:74074-86-5
Molecular Formula:C₁₅H₂₀O₄S₃
Molecular Weight:360.519
Hs Code.:

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Chemical Property of ethoxycarbonylmethyl 2-methyl-2-(p-tolylsulfonyl)propanedithioate

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Technology Process of ethoxycarbonylmethyl 2-methyl-2-(p-tolylsulfonyl)propanedithioate

There total 3 articles about ethoxycarbonylmethyl 2-methyl-2-(p-tolylsulfonyl)propanedithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 75-15-0,12122-00-8
carbon disulfide

: 51751-71-4,20288-47-5
1-methyl-4-(propane-2-sulfonyl)benzene

: 105-36-2
ethyl bromoacetate

: 74074-86-5
ethoxycarbonylmethyl 2-methyl-2-(p-tolylsulfonyl)propanedithioate

Guidance literature:: With methyllithium; In tetrahydrofuran; for 0.5h; Ambient temperature;

Reference yield:

: 14905-81-8
1-(isopropylthio)-4-methylbenzene

: 74074-86-5
ethoxycarbonylmethyl 2-methyl-2-(p-tolylsulfonyl)propanedithioate

Guidance literature:: Multi-step reaction with 2 steps

1: 30percent H₂O₂ / acetic acid

2: 41 percent / MeLi / tetrahydrofuran / 0.5 h / Ambient temperature

With methyllithium; dihydrogen peroxide; In tetrahydrofuran; acetic acid;

Reference yield:

: 106-45-6
para-thiocresol

: 74074-86-5
ethoxycarbonylmethyl 2-methyl-2-(p-tolylsulfonyl)propanedithioate

Guidance literature:: Multi-step reaction with 3 steps

2: 30percent H₂O₂ / acetic acid

3: 41 percent / MeLi / tetrahydrofuran / 0.5 h / Ambient temperature

With methyllithium; dihydrogen peroxide; In tetrahydrofuran; acetic acid;