C₂₃H₁₉BrClF₃N₆O₃S

Base Information

Chemical Name:C₂₃H₁₉BrClF₃N₆O₃S
CAS No.:1352547-96-6
Molecular Formula:C₂₃H₁₉BrClF₃N₆O₃S
Molecular Weight:631.86
Hs Code.:

C<sub>23</sub>H<sub>19</sub>BrClF<sub>3</sub>N<sub>6</sub>O<sub>3</sub>S

Synonyms:

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Chemical Property of C₂₃H₁₉BrClF₃N₆O₃S

Chemical Property:

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Technology Process of C₂₃H₁₉BrClF₃N₆O₃S

There total 9 articles about C₂₃H₁₉BrClF₃N₆O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 22841-92-5
(3-chloro-2-pyridyl)hydrazine

: 1352547-96-6
C₂₃H₁₉BrClF₃N₆O₃S

Guidance literature:: Multi-step reaction with 7 steps

1: sodium ethanolate / ethanol / Reflux

2: dipotassium peroxodisulfate; sulfuric acid / acetonitrile / Reflux

3: potassium carbonate / N,N-dimethyl-formamide / 100 °C

4: sodium hydroxide / water; methanol

5: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 20 °C

6: polyethylene glycol-400 / acetonitrile / 0.67 h / 20 °C

7: acetonitrile / 20 °C

With dipotassium peroxodisulfate; oxalyl dichloride; sulfuric acid; sodium ethanolate; potassium carbonate; N,N-dimethyl-formamide; sodium hydroxide; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jf4012467

Reference yield:

: 500011-88-1
2-(3-chloro-pyridin-2-yl)-5-oxo-pyrazolidine-3-carboxylic acid ethyl ester

: 1352547-96-6
C₂₃H₁₉BrClF₃N₆O₃S

Guidance literature:: Multi-step reaction with 6 steps

1: dipotassium peroxodisulfate; sulfuric acid / acetonitrile / Reflux

2: potassium carbonate / N,N-dimethyl-formamide / 100 °C

3: sodium hydroxide / water; methanol

4: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 20 °C

5: polyethylene glycol-400 / acetonitrile / 0.67 h / 20 °C

6: acetonitrile / 20 °C

With dipotassium peroxodisulfate; oxalyl dichloride; sulfuric acid; potassium carbonate; N,N-dimethyl-formamide; sodium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jf4012467

Reference yield:

: 500011-95-0
2-(3-chloro-pyridin-2-yl)-5-oxo-2,5-dihydro-1H-pyrazole-3-carboxylic acid ethyl ester

: 1352547-96-6
C₂₃H₁₉BrClF₃N₆O₃S

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 100 °C

2: sodium hydroxide / water; methanol

3: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 3 h / 20 °C

4: polyethylene glycol-400 / acetonitrile / 0.67 h / 20 °C

5: acetonitrile / 20 °C

With oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; sodium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jf4012467