11-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3,9-bis-O-[tert-butyl(dimethyl)silyl]-2,4,6,8,10-pentadeoxy-1-O-(3,4-dimethoxybenzyl)-4-methyl-5,7-O-(oxomethylene)-D-glycero-D-gluco-undecitol

Base Information

Chemical Name:11-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3,9-bis-O-[tert-butyl(dimethyl)silyl]-2,4,6,8,10-pentadeoxy-1-O-(3,4-dimethoxybenzyl)-4-methyl-5,7-O-(oxomethylene)-D-glycero-D-gluco-undecitol
CAS No.:1428672-02-9
Molecular Formula:C₅₅H₈₀O₁₁Si₂
Molecular Weight:973.405
Hs Code.:

11-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3,9-bis-O-[tert-butyl(dimethyl)silyl]-2,4,6,8,10-pentadeoxy-1-O-(3,4-dimethoxybenzyl)-4-methyl-5,7-O-(oxomethylene)-D-glycero-D-gluco-undecitol

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Chemical Property of 11-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3,9-bis-O-[tert-butyl(dimethyl)silyl]-2,4,6,8,10-pentadeoxy-1-O-(3,4-dimethoxybenzyl)-4-methyl-5,7-O-(oxomethylene)-D-glycero-D-gluco-undecitol

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Technology Process of 11-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3,9-bis-O-[tert-butyl(dimethyl)silyl]-2,4,6,8,10-pentadeoxy-1-O-(3,4-dimethoxybenzyl)-4-methyl-5,7-O-(oxomethylene)-D-glycero-D-gluco-undecitol

There total 3 articles about 11-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3,9-bis-O-[tert-butyl(dimethyl)silyl]-2,4,6,8,10-pentadeoxy-1-O-(3,4-dimethoxybenzyl)-4-methyl-5,7-O-(oxomethylene)-D-glycero-D-gluco-undecitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428672-00-7
C₅₆H₈₆O₉Si₃

: 1428672-02-9
11-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3,9-bis-O-[tert-butyl(dimethyl)silyl]-2,4,6,8,10-pentadeoxy-1-O-(3,4-dimethoxybenzyl)-4-methyl-5,7-O-(oxomethylene)-D-glycero-D-gluco-undecitol

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; potassium hydrogencarbonate / methanol; tetrahydrofuran

2: toluene / 2 h / 110 °C

With dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/ja401918r

Reference yield:

: 1428671-98-0
(5S,6S,7R,9Z,11R)-11-{2-[bis(4-methoxyphenyl)(phenyl)methoxy]ethyl}-5-{2-[(3,4-dimethoxybenzyl)oxy]ethyl}-2,2,3,3,6,13,13,14,14-nonamethyl-4,12-dioxa-3,13-disilapentadec-9-en-7-ol

: 1428672-02-9
11-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3,9-bis-O-[tert-butyl(dimethyl)silyl]-2,4,6,8,10-pentadeoxy-1-O-(3,4-dimethoxybenzyl)-4-methyl-5,7-O-(oxomethylene)-D-glycero-D-gluco-undecitol

Guidance literature:: Multi-step reaction with 4 steps

1: 20 °C

2: toluene / 3 h / 0 °C

3: dihydrogen peroxide; potassium hydrogencarbonate / methanol; tetrahydrofuran

4: toluene / 2 h / 110 °C

With dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/ja401918r

Reference yield:

: 1428671-99-1
C₅₆H₈₆O₉Si₃

: 1428672-02-9
11-O-[bis(4-methoxyphenyl)(phenyl)methyl]-3,9-bis-O-[tert-butyl(dimethyl)silyl]-2,4,6,8,10-pentadeoxy-1-O-(3,4-dimethoxybenzyl)-4-methyl-5,7-O-(oxomethylene)-D-glycero-D-gluco-undecitol

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 3 h / 0 °C

2: dihydrogen peroxide; potassium hydrogencarbonate / methanol; tetrahydrofuran

3: toluene / 2 h / 110 °C

With dihydrogen peroxide; potassium hydrogencarbonate; In tetrahydrofuran; methanol; toluene;
DOI:10.1021/ja401918r