tert-butyl 2,2'2'',2'''-[2,2'-(2,2'-[2,2'-(2,5-diiodo-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl)]bis(oxy)bis(ethane-2,1-diyl))bis(oxy)bis(ethane-2,1-diyl)]bis(azanetriyl)tetrakis(ethane-2,1-diyl)tetracarbamate

Base Information

Chemical Name:tert-butyl 2,2'2'',2'''-[2,2'-(2,2'-[2,2'-(2,5-diiodo-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl)]bis(oxy)bis(ethane-2,1-diyl))bis(oxy)bis(ethane-2,1-diyl)]bis(azanetriyl)tetrakis(ethane-2,1-diyl)tetracarbamate
CAS No.:1445733-77-6
Molecular Formula:C₄₆H₈₂I₂N₆O₁₄
Molecular Weight:1197
Hs Code.:

tert-butyl 2,2'2'',2'''-[2,2'-(2,2'-[2,2'-(2,5-diiodo-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl)]bis(oxy)bis(ethane-2,1-diyl))bis(oxy)bis(ethane-2,1-diyl)]bis(azanetriyl)tetrakis(ethane-2,1-diyl)tetracarbamate

Synonyms:

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Chemical Property of tert-butyl 2,2'2'',2'''-[2,2'-(2,2'-[2,2'-(2,5-diiodo-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl)]bis(oxy)bis(ethane-2,1-diyl))bis(oxy)bis(ethane-2,1-diyl)]bis(azanetriyl)tetrakis(ethane-2,1-diyl)tetracarbamate

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Technology Process of tert-butyl 2,2'2'',2'''-[2,2'-(2,2'-[2,2'-(2,5-diiodo-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl)]bis(oxy)bis(ethane-2,1-diyl))bis(oxy)bis(ethane-2,1-diyl)]bis(azanetriyl)tetrakis(ethane-2,1-diyl)tetracarbamate

There total 4 articles about tert-butyl 2,2'2'',2'''-[2,2'-(2,2'-[2,2'-(2,5-diiodo-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl)]bis(oxy)bis(ethane-2,1-diyl))bis(oxy)bis(ethane-2,1-diyl)]bis(azanetriyl)tetrakis(ethane-2,1-diyl)tetracarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1445733-76-5
1,4-bis(2-(2-(2-chloroethoxy)ethoxy)ethoxy)-2,5-diiodobenzene

: 117499-16-8
bis(2-tert-butyloxycarbonylaminoethyl)amine

: 1445733-77-6
tert-butyl 2,2'2'',2'''-[2,2'-(2,2'-[2,2'-(2,5-diiodo-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl)]bis(oxy)bis(ethane-2,1-diyl))bis(oxy)bis(ethane-2,1-diyl)]bis(azanetriyl)tetrakis(ethane-2,1-diyl)tetracarbamate

Guidance literature:: With potassium carbonate; In acetonitrile; for 72h; Reflux;
DOI:10.1039/c3cc43015d

Reference yield:

: 108213-17-8
2-(2-(2-chloroethoxy)ethoxy)ethyl 4-methylbenzenesulfonate

: 1445733-77-6
tert-butyl 2,2'2'',2'''-[2,2'-(2,2'-[2,2'-(2,5-diiodo-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl)]bis(oxy)bis(ethane-2,1-diyl))bis(oxy)bis(ethane-2,1-diyl)]bis(azanetriyl)tetrakis(ethane-2,1-diyl)tetracarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / butanone / 24 h / Reflux

2: potassium carbonate / acetonitrile / 72 h / Reflux

With potassium carbonate; In acetonitrile; butanone;
DOI:10.1039/c3cc43015d

Reference yield:

: 58632-95-4
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile

: 1445733-77-6
tert-butyl 2,2'2'',2'''-[2,2'-(2,2'-[2,2'-(2,5-diiodo-1,4-phenylene)bis(oxy)bis(ethane-2,1-diyl)]bis(oxy)bis(ethane-2,1-diyl))bis(oxy)bis(ethane-2,1-diyl)]bis(azanetriyl)tetrakis(ethane-2,1-diyl)tetracarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 3 h / 0 °C

2: potassium carbonate / acetonitrile / 72 h / Reflux

With potassium carbonate; triethylamine; In tetrahydrofuran; acetonitrile;
DOI:10.1039/c3cc43015d