C₂₂H₂₉N₅O₆S

Base Information

Chemical Name:C₂₂H₂₉N₅O₆S
CAS No.:1053650-83-1
Molecular Formula:C₂₂H₂₉N₅O₆S
Molecular Weight:491.568
Hs Code.:

C<sub>22</sub>H<sub>29</sub>N<sub>5</sub>O<sub>6</sub>S

Synonyms:

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Chemical Property of C₂₂H₂₉N₅O₆S

Chemical Property:

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Technology Process of C₂₂H₂₉N₅O₆S

There total 8 articles about C₂₂H₂₉N₅O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2480-93-5
Boc-Orn(Z)-OH

: 1053650-83-1
C₂₂H₂₉N₅O₆S

Guidance literature:: Multi-step reaction with 9 steps

1.1: ethyl chloroformate / tetrahydrofuran / 0.25 h / -10 - 0 °C

1.2: 83 percent / NaBH₄ / tetrahydrofuran; methanol / 0 °C

2.1: 80 percent / triethylamine / CH₂Cl₂ / 1.5 h / 0 - 20 °C

3.1: 69 percent / Cs₂CO₃ / dimethylformamide / 0 °C

4.1: sulfuryl chloride; acetic anhydride / CH₂Cl₂ / 1 h / -20 - -5 °C

5.1: 73 percent / NH₃ / CH₂Cl₂ / 0.25 h / -10 °C

6.1: 85 percent / NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0.75 h / 0 - 20 °C

7.1: hydrogen / 10percent Pd/C / ethanol / 4 h

8.1: 230 mg / tetrahydrofuran

9.1: TFA / CH₂Cl₂ / 0.5 h / 0 °C

With sodium periodate; sulfuryl dichloride; ammonia; hydrogen; chloroformic acid ethyl ester; acetic anhydride; caesium carbonate; triethylamine; trifluoroacetic acid; ruthenium trichloride; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1.1: Substitution / 1.2: Reduction / 2.1: Substitution / 3.1: Substitution / 4.1: Deacetylation / 5.1: Substitution / 6.1: Oxidation / 7.1: Hydrogenolysis / 8.1: Substitution / 9.1: Hydrolysis;
DOI:10.1002/1099-0690(200004)2000:7<1219::AID-EJOC1219>3.0.CO;2-P

Reference yield:

: 105562-75-2
N²-(tert-butyloxycarbonyl)-N⁵-(benzyloxycarbonyl)-2(S),5-diaminopentanol

: 1053650-83-1
C₂₂H₂₉N₅O₆S

Guidance literature:: Multi-step reaction with 8 steps

1: 80 percent / triethylamine / CH₂Cl₂ / 1.5 h / 0 - 20 °C

2: 69 percent / Cs₂CO₃ / dimethylformamide / 0 °C

3: sulfuryl chloride; acetic anhydride / CH₂Cl₂ / 1 h / -20 - -5 °C

4: 73 percent / NH₃ / CH₂Cl₂ / 0.25 h / -10 °C

5: 85 percent / NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0.75 h / 0 - 20 °C

6: hydrogen / 10percent Pd/C / ethanol / 4 h

7: 230 mg / tetrahydrofuran

8: TFA / CH₂Cl₂ / 0.5 h / 0 °C

With sodium periodate; sulfuryl dichloride; ammonia; hydrogen; acetic anhydride; caesium carbonate; triethylamine; trifluoroacetic acid; ruthenium trichloride; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1: Substitution / 2: Substitution / 3: Deacetylation / 4: Substitution / 5: Oxidation / 6: Hydrogenolysis / 7: Substitution / 8: Hydrolysis;
DOI:10.1002/1099-0690(200004)2000:7<1219::AID-EJOC1219>3.0.CO;2-P

Reference yield:

: 233689-90-2
Boc-NH-CH((CH₂)3NHZ)-CH₂-S-CO-CH₃

: 1053650-83-1
C₂₂H₂₉N₅O₆S

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuryl chloride; acetic anhydride / CH₂Cl₂ / 1 h / -20 - -5 °C

2: 73 percent / NH₃ / CH₂Cl₂ / 0.25 h / -10 °C

3: 85 percent / NaIO₄ / RuCl₃*H₂O / CH₂Cl₂; acetonitrile; H₂O / 0.75 h / 0 - 20 °C

4: hydrogen / 10percent Pd/C / ethanol / 4 h

5: 230 mg / tetrahydrofuran

6: TFA / CH₂Cl₂ / 0.5 h / 0 °C

With sodium periodate; sulfuryl dichloride; ammonia; hydrogen; acetic anhydride; trifluoroacetic acid; ruthenium trichloride; In tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile; 1: Deacetylation / 2: Substitution / 3: Oxidation / 4: Hydrogenolysis / 5: Substitution / 6: Hydrolysis;
DOI:10.1002/1099-0690(200004)2000:7<1219::AID-EJOC1219>3.0.CO;2-P