RuCl(P(C₆H₄)(C₆H₅)2)(P(C₆H₅)3)2*CH₂Cl₂

Base Information

Chemical Name:RuCl(P(C₆H₄)(C₆H₅)2)(P(C₆H₅)3)2*CH₂Cl₂
CAS No.:82008-46-6
Molecular Formula:CH₂Cl₂*C₅₄H₄₄ClP₃Ru
Molecular Weight:1007.32
Hs Code.:

RuCl(P(C<sub>6</sub>H<sub>4</sub>)(C<sub>6</sub>H<sub>5</sub>)2)(P(C<sub>6</sub>H<sub>5</sub>)3)2*CH<sub>2</sub>Cl<sub>2</sub>

Synonyms:

Suppliers and Price of RuCl(P(C₆H₄)(C₆H₅)2)(P(C₆H₅)3)2*CH₂Cl₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of RuCl(P(C₆H₄)(C₆H₅)2)(P(C₆H₅)3)2*CH₂Cl₂

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Technology Process of RuCl(P(C₆H₄)(C₆H₅)2)(P(C₆H₅)3)2*CH₂Cl₂

There total 2 articles about RuCl(P(C₆H₄)(C₆H₅)2)(P(C₆H₅)3)2*CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 55102-19-7
hydridochlorotris(triphenylphosphine)ruthenium(II)

: 928-49-4
hex-3-yne

: 82008-46-6
RuCl(P(C₆H₄)(C₆H₅)2)(P(C₆H₅)3)2*CH₂Cl₂

Guidance literature:: In dichloromethane; byproducts: triphenylphosphine; 4 equiv of the alkyne adding with stirring to a soln. of the hydride complex under Ar or N2, stirring for 90 min, an equal volume of pentane adding, cooling to -40°C, after 36 h solid was collecting, washing with pentane; iodentified by elem. anal. and NMR spectra;

Reference yield:

: 15529-49-4,41756-81-4
tris(triphenylphosphine)ruthenium(II) chloride

: 12636-72-5
bis(cyclopentadienyl)dimethylzirconium(IV)

: zirconocene methyl chloride

: 82008-46-6
RuCl(C₆H₄P(C₆H₅)2)(P(C₆H₅)3)2

Guidance literature:: In toluene; byproducts: methane; Electrochem. Process; stopping react. between stoich. amts. of Ru-compd. and Zr-compd. in toluene as soon as the gas evolution of CH4 is finished;

Reference yield:

: 82008-46-6
RuCl(P(C₆H₄)(C₆H₅)2)(P(C₆H₅)3)2*CH₂Cl₂

: 16873-17-9,12184-84-8
deuterium

: 97749-31-0
Ru⁽²⁾HCl(P(C₆H₃⁽²⁾H₂)3)3

Guidance literature:: In toluene; repeated equilibration of the complex with fresh portions of D2 gas at 75°C; identified by (1)H and (2)H NMR spectra;