2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol

Base Information

Chemical Name:2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol
CAS No.:93292-80-9
Molecular Formula:C₃₅H₅₄O₈
Molecular Weight:602.809
Hs Code.:

2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol

Synonyms:

Suppliers and Price of 2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol

There total 9 articles about 2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 93381-42-1
(1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol

: 93292-80-9
2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol

Guidance literature:: With lithium-n-butanethiolate; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 100 ℃; Yield given;
DOI:10.1016/0040-4039(84)80039-8

Reference yield:

: 17269-81-7
2-bromo-6-(2-propenyl)phenol

: 93292-80-9
2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol

Guidance literature:: Multi-step reaction with 8 steps

1: 88 percent / KOt-Bu / 2-methyl-propan-2-ol

2: basic alumina (Woelm, akt I) / hexane; ethyl acetate / by eluting through a column

3: O₃

4: m-chloroperbenzoic acid / CH₂Cl₂

6: 69 percent / t-butyllithium, copper iodide, tri-n-butylphosphine / diethyl ether / -78 °C

7: NaBH₄ / methanol

8: lithium n-butyl mercaptide / hexamethylphosphoric acid triamide / 100 °C

With aluminum oxide; sodium tetrahydroborate; copper(l) iodide; tributylphosphine; potassium tert-butylate; tert.-butyl lithium; lithium-n-butanethiolate; ozone; 3-chloro-benzenecarboperoxoic acid; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; hexane; dichloromethane; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/0040-4039(84)80039-8

Reference yield:

: 88275-72-3
3-Brom-2-methoxy-1-(2-propenyl)benzol

: 93292-80-9
2-{(1R,2R,3R,5R)-5-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-2-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentylmethyl}-6-(tetrahydro-pyran-2-yloxy)-phenol

Guidance literature:: Multi-step reaction with 7 steps

1: basic alumina (Woelm, akt I) / hexane; ethyl acetate / by eluting through a column

2: O₃

3: m-chloroperbenzoic acid / CH₂Cl₂

5: 69 percent / t-butyllithium, copper iodide, tri-n-butylphosphine / diethyl ether / -78 °C

6: NaBH₄ / methanol

7: lithium n-butyl mercaptide / hexamethylphosphoric acid triamide / 100 °C

With aluminum oxide; sodium tetrahydroborate; copper(l) iodide; tributylphosphine; tert.-butyl lithium; lithium-n-butanethiolate; ozone; 3-chloro-benzenecarboperoxoic acid; In methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; diethyl ether; hexane; dichloromethane; ethyl acetate;
DOI:10.1016/0040-4039(84)80039-8