(1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol

Base Information

Chemical Name:(1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol
CAS No.:93381-42-1
Molecular Formula:C₃₆H₅₆O₈
Molecular Weight:616.836
Hs Code.:

(1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol

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Chemical Property of (1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol

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Technology Process of (1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol

There total 9 articles about (1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17269-81-7
2-bromo-6-(2-propenyl)phenol

: 93381-42-1
(1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol

Guidance literature:: Multi-step reaction with 7 steps

1: 88 percent / KOt-Bu / 2-methyl-propan-2-ol

2: basic alumina (Woelm, akt I) / hexane; ethyl acetate / by eluting through a column

3: O₃

4: m-chloroperbenzoic acid / CH₂Cl₂

6: 69 percent / t-butyllithium, copper iodide, tri-n-butylphosphine / diethyl ether / -78 °C

7: NaBH₄ / methanol

With aluminum oxide; sodium tetrahydroborate; copper(l) iodide; tributylphosphine; potassium tert-butylate; tert.-butyl lithium; ozone; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; hexane; dichloromethane; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/0040-4039(84)80039-8

Reference yield:

: 88275-72-3
3-Brom-2-methoxy-1-(2-propenyl)benzol

: 93381-42-1
(1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol

Guidance literature:: Multi-step reaction with 6 steps

1: basic alumina (Woelm, akt I) / hexane; ethyl acetate / by eluting through a column

2: O₃

3: m-chloroperbenzoic acid / CH₂Cl₂

5: 69 percent / t-butyllithium, copper iodide, tri-n-butylphosphine / diethyl ether / -78 °C

6: NaBH₄ / methanol

With aluminum oxide; sodium tetrahydroborate; copper(l) iodide; tributylphosphine; tert.-butyl lithium; ozone; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; hexane; dichloromethane; ethyl acetate;
DOI:10.1016/0040-4039(84)80039-8

Reference yield:

: 88275-87-0
3-bromo-2-methyloxybenzaldehyde

: 93381-42-1
(1R,2R,3R,4R)-2-[2-Methoxy-3-(tetrahydro-pyran-2-yloxy)-benzyl]-4-(tetrahydro-pyran-2-yloxy)-3-[(E)-(S)-3-(tetrahydro-pyran-2-yloxy)-oct-1-enyl]-cyclopentanol

Guidance literature:: Multi-step reaction with 4 steps

1: m-chloroperbenzoic acid / CH₂Cl₂

3: 69 percent / t-butyllithium, copper iodide, tri-n-butylphosphine / diethyl ether / -78 °C

4: NaBH₄ / methanol

With sodium tetrahydroborate; copper(l) iodide; tributylphosphine; tert.-butyl lithium; 3-chloro-benzenecarboperoxoic acid; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/0040-4039(84)80039-8