4,6-dihydroxy-2,3-dimethylacetophenone

Base Information

Chemical Name:4,6-dihydroxy-2,3-dimethylacetophenone
CAS No.:7743-14-8
Molecular Formula:C₁₀H₁₂O₃
Molecular Weight:180.203
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,6-dihydroxy-2,3-dimethylacetophenone

Chemical Property:

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Technology Process of 4,6-dihydroxy-2,3-dimethylacetophenone

There total 4 articles about 4,6-dihydroxy-2,3-dimethylacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7149-90-8
2,4-dimethoxy-6-methyl-benzaldehyde

: 7743-14-8
4,6-dihydroxy-2,3-dimethylacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1: KOH; triethylene glycol; hydrazine hydrate / 185 °C

2: aqueous HBr

3: ZnCl₂; diethyl ether / Erhitzen des Reaktionsprodukts mit Wasser

With potassium hydroxide; diethyl ether; hydrogen bromide; hydrazine hydrate; zinc(II) chloride; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol;
DOI:10.1021/ja01192a078

Reference yield:

: 59968-26-2
1,3-dimethoxy-5,6-dimethylbenzene

: 7743-14-8
4,6-dihydroxy-2,3-dimethylacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous HBr

2: ZnCl₂; diethyl ether / Erhitzen des Reaktionsprodukts mit Wasser

With diethyl ether; hydrogen bromide; zinc(II) chloride;
DOI:10.1021/ja01192a078