Imidazole-1-carbothioic acid O-{(S)-1-[(4R,5S,6R)-6-benzyl-1,3-bis-cyclopropylmethyl-5-(2-methoxy-ethoxymethoxy)-2-oxo-hexahydro-pyrimidin-4-yl]-2-phenyl-ethyl} ester

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Chemical Name:Imidazole-1-carbothioic acid O-{(S)-1-[(4R,5S,6R)-6-benzyl-1,3-bis-cyclopropylmethyl-5-(2-methoxy-ethoxymethoxy)-2-oxo-hexahydro-pyrimidin-4-yl]-2-phenyl-ethyl} ester
CAS No.:210635-03-3
Molecular Formula:C₃₅H₄₄N₄O₅S
Molecular Weight:632.824
Hs Code.:

Imidazole-1-carbothioic acid O-{(S)-1-[(4R,5S,6R)-6-benzyl-1,3-bis-cyclopropylmethyl-5-(2-methoxy-ethoxymethoxy)-2-oxo-hexahydro-pyrimidin-4-yl]-2-phenyl-ethyl} ester

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Chemical Property of Imidazole-1-carbothioic acid O-{(S)-1-[(4R,5S,6R)-6-benzyl-1,3-bis-cyclopropylmethyl-5-(2-methoxy-ethoxymethoxy)-2-oxo-hexahydro-pyrimidin-4-yl]-2-phenyl-ethyl} ester

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Technology Process of Imidazole-1-carbothioic acid O-{(S)-1-[(4R,5S,6R)-6-benzyl-1,3-bis-cyclopropylmethyl-5-(2-methoxy-ethoxymethoxy)-2-oxo-hexahydro-pyrimidin-4-yl]-2-phenyl-ethyl} ester

There total 3 articles about Imidazole-1-carbothioic acid O-{(S)-1-[(4R,5S,6R)-6-benzyl-1,3-bis-cyclopropylmethyl-5-(2-methoxy-ethoxymethoxy)-2-oxo-hexahydro-pyrimidin-4-yl]-2-phenyl-ethyl} ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 152929-98-1
(4R,5S,6S,7R)-hexahydro-5-(2-methoxyethoxymethoxy)-6-hydroxy-1,3-bis--4,7-bis--2H-1,3-diazepin-2-one

: 210635-03-3
Imidazole-1-carbothioic acid O-{(S)-1-[(4R,5S,6R)-6-benzyl-1,3-bis-cyclopropylmethyl-5-(2-methoxy-ethoxymethoxy)-2-oxo-hexahydro-pyrimidin-4-yl]-2-phenyl-ethyl} ester

Guidance literature:: Multi-step reaction with 3 steps

1: 0.9 g / DEAD, Ph₃P / tetrahydrofuran / 20 h / Ambient temperature

2: 0.4 g / aq. NaOH / methanol / 1 h / Ambient temperature

3: 34 mg / tetrahydrofuran / 4 h / Heating

With sodium hydroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol;
DOI:10.1021/jo980533e

Reference yield:

: 210635-00-0
Chloro-acetic acid (S)-1-[(4R,5S,6R)-6-benzyl-1,3-bis-cyclopropylmethyl-5-(2-methoxy-ethoxymethoxy)-2-oxo-hexahydro-pyrimidin-4-yl]-2-phenyl-ethyl ester

: 210635-03-3
Imidazole-1-carbothioic acid O-{(S)-1-[(4R,5S,6R)-6-benzyl-1,3-bis-cyclopropylmethyl-5-(2-methoxy-ethoxymethoxy)-2-oxo-hexahydro-pyrimidin-4-yl]-2-phenyl-ethyl} ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.4 g / aq. NaOH / methanol / 1 h / Ambient temperature

2: 34 mg / tetrahydrofuran / 4 h / Heating

With sodium hydroxide; In tetrahydrofuran; methanol;
DOI:10.1021/jo980533e