allaric acid bis-(N'-phenyl-hydrazide)

Base Information

• Chemical Name: allaric acid bis-(N'-phenyl-hydrazide)
• CAS No.: 113973-60-7
• Molecular Formula: C₁₈H₂₂N₄O₆
• Molecular Weight: 390.396
• Mol file: 113973-60-7.mol

Synonyms:

Chemical Property of allaric acid bis-(N'-phenyl-hydrazide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of allaric acid bis-(N'-phenyl-hydrazide)

There total 3 articles about allaric acid bis-(N'-phenyl-hydrazide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetra-O-acetyl-allo-mucic dialdehyde (113973-56-1) → allaric acid bis-(N'-phenyl-hydrazide) (113973-60-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 82.5 percent / perpropionic acid / propionic acid / Ambient temperature

2: H₂O

With perpropionic acid; In water; propionic acid;

DOI:10.1016/0008-6215(87)80140-4

Reference yield:

tetra-O-acetyl-galactaric acid bis-(N'-phenyl-hydrazide) (124359-98-4) + sodium methylate (124-41-4) → galactaric acid bis-(N'-phenyl-hydrazide) (7404-38-8,99782-61-3,110507-66-9,113973-60-7)

Guidance literature:

DOI:10.1021/ja01556a041

Reference yield:

tetra-O-acetyl-allo-mucic acid (113973-57-2) + phenylhydrazine (100-63-0) → allaric acid bis-(N'-phenyl-hydrazide) (113973-60-7)

Guidance literature:

In water;

DOI:10.1016/0008-6215(87)80140-4

upstream raw materials:

tetra-O-acetyl-allo-mucic acid

phenylhydrazine

tetra-O-acetyl-allo-mucic dialdehyde

tetra-O-acetyl-galactaric acid bis-(N'-phenyl-hydrazide)

Refernces