N-[2-Methoxy-2-(4-methoxyphenyl)ethyl]cinnamide

Base Information

Chemical Name:N-[2-Methoxy-2-(4-methoxyphenyl)ethyl]cinnamide
CAS No.:70546-93-9
Molecular Formula:C₁₉H₂₁NO₃
Molecular Weight:311.381
Hs Code.:
NSC Number:711466
DSSTox Substance ID:DTXSID801164027
Nikkaji Number:J3.526.302K
Metabolomics Workbench ID:48604

Synonyms:N-[2-Methoxy-2-(4-methoxyphenyl)ethyl]cinnamide;NSC711466;Aegle marmelos Alkaloid D;DTXSID801164027;NSC-711466;J3.526.302K;N-[2-(4-Methoxyphenyl)-2-methoxyethyl]-3-phenylacrylamide;(2E)-N-[2-Methoxy-2-(4-methoxyphenyl)ethyl]-3-phenyl-2-propenamide;(2E)-N-[2-methoxy-2-(4-methoxyphenyl)ethyl]-3-phenylprop-2-enamide;70546-93-9

Suppliers and Price of N-[2-Methoxy-2-(4-methoxyphenyl)ethyl]cinnamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of N-[2-Methoxy-2-(4-methoxyphenyl)ethyl]cinnamide

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:311.15214353
Heavy Atom Count:23
Complexity:369

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C(CNC(=O)C=CC2=CC=CC=C2)OC
Isomeric SMILES:COC1=CC=C(C=C1)C(CNC(=O)/C=C/C2=CC=CC=C2)OC

Technology Process of N-[2-Methoxy-2-(4-methoxyphenyl)ethyl]cinnamide

There total 3 articles about N-[2-Methoxy-2-(4-methoxyphenyl)ethyl]cinnamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31367-42-7
2-(p-methoxyphenyl)-2-methoxyethylamine

: 102-92-1,17082-09-6
cinnamoyl chloride

: 70546-93-9
N-[2-methoxy-2-(4-methoxyphenyl)ethyl]-3-phenyl-2-propenamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 25 ℃; for 2.16667h;
DOI:10.1002/anie.201507630

Reference yield:

: 637-69-4,24936-44-5
4-Methoxystyrene

: 70546-93-9
N-[2-methoxy-2-(4-methoxyphenyl)ethyl]-3-phenyl-2-propenamide

Guidance literature:: Multi-step reaction with 2 steps

1: O-pivaloylhydroxylamine trifluoromethanesulfonate salt; (phthalocyaninato)iron(II) / 16 h / 25 °C / Inert atmosphere

2: triethylamine / dichloromethane / 2.17 h / 0 - 25 °C

With (phthalocyaninato)iron(II); O-pivaloylhydroxylamine trifluoromethanesulfonate salt; triethylamine; In dichloromethane;
DOI:10.1002/anie.201507630