2,2',2''-(10-(2-(4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)phenylamino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)tris(N,N-dimethylacetamide)

Base Information

Chemical Name:2,2',2''-(10-(2-(4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)phenylamino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)tris(N,N-dimethylacetamide)
CAS No.:1367372-03-9
Molecular Formula:C₃₂H₄₉N₉O₆
Molecular Weight:655.798
Hs Code.:

2,2',2''-(10-(2-(4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)phenylamino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)tris(N,N-dimethylacetamide)

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Chemical Property of 2,2',2''-(10-(2-(4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)phenylamino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)tris(N,N-dimethylacetamide)

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Technology Process of 2,2',2''-(10-(2-(4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)phenylamino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)tris(N,N-dimethylacetamide)

There total 4 articles about 2,2',2''-(10-(2-(4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)phenylamino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)tris(N,N-dimethylacetamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 951238-19-0
2-{4,7-bis-dimethylcarbamoylmethyl-10-[(4-nitro-phenylcarbamoyl)-methyl]-1,4,7,10-tetraaza-cyclododec-1-yl}-N,N-dimethyl-acetamide

: 1367372-03-9
2,2',2''-(10-(2-(4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)phenylamino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)tris(N,N-dimethylacetamide)

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrazine hydrate / ethanol / 2 h / 80 °C / Microwave irradiation

2: acetonitrile / 24 h / 85 °C

3: sodium acetate; acetic anhydride / 2 h / 100 °C

With palladium 10% on activated carbon; sodium acetate; acetic anhydride; hydrazine hydrate; In ethanol; acetonitrile;
DOI:10.1021/ja300887k

Reference yield:

: 951238-20-3
2-{4[(4-amino-phenylcarbamoyl)-methyl]-7,10-(bis-dimethylcarbamoylmethyl-1,4,7,10-tetraaza-cyclododec-1-yl)}-N,N-dimethyl-acetamide

: 1367372-03-9
2,2',2''-(10-(2-(4-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)phenylamino)-2-oxoethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)tris(N,N-dimethylacetamide)

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 24 h / 85 °C

2: sodium acetate; acetic anhydride / 2 h / 100 °C

With sodium acetate; acetic anhydride; In acetonitrile;
DOI:10.1021/ja300887k