Phosphine oxide, (4,6-dimethyl-1,3-dioxan-2-yl)diphenyl-, (2alpha,4alpha,6alpha)-

Base Information

Chemical Name:Phosphine oxide, (4,6-dimethyl-1,3-dioxan-2-yl)diphenyl-, (2alpha,4alpha,6alpha)-
CAS No.:130506-61-5
Molecular Formula:C₁₈H₂₁O₃P
Molecular Weight:316.337
Hs Code.:
DSSTox Substance ID:DTXSID801157282

Synonyms:DTXSID801157282;Phosphine oxide, (4,6-dimethyl-1,3-dioxan-2-yl)diphenyl-, (2alpha,4alpha,6alpha)-;130506-61-5

Suppliers and Price of Phosphine oxide, (4,6-dimethyl-1,3-dioxan-2-yl)diphenyl-, (2alpha,4alpha,6alpha)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Phosphine oxide, (4,6-dimethyl-1,3-dioxan-2-yl)diphenyl-, (2alpha,4alpha,6alpha)-

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:316.12283153
Heavy Atom Count:22
Complexity:367

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1CC(OC(O1)P(=O)(C2=CC=CC=C2)C3=CC=CC=C3)C
Isomeric SMILES:C[C@@H]1C[C@@H](OC(O1)P(=O)(C2=CC=CC=C2)C3=CC=CC=C3)C

Technology Process of Phosphine oxide, (4,6-dimethyl-1,3-dioxan-2-yl)diphenyl-, (2alpha,4alpha,6alpha)-

There total 3 articles about Phosphine oxide, (4,6-dimethyl-1,3-dioxan-2-yl)diphenyl-, (2alpha,4alpha,6alpha)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.4%

: 27350-46-5
isopropyl diphenylphosphinite

: 142572-28-9,142632-72-2
(cis-4,6-Dimethyl-1,3-dioxan-2-yl)trimethylammonium iodide

: 142632-71-1
r-2-Diphenylphosphinoyl-t-4,t-6-dimethyl-1,3-dioxane

: 130506-61-5
r-2-Diphenylphosphinoyl-c-4,c-6-dimethyl-1,3-dioxane

Guidance literature:: In toluene; for 3h; Yields of byproduct given; Heating;
DOI:10.1016/S0040-4020(01)92198-2

Reference yield: 14.8%

: 20570-20-1
(Diethoxymethyl)diphenylphosphine oxide

: 1825-14-5,3950-21-8,36402-52-5,42075-32-1,72345-23-4,625-69-4
pentane-1,3-diol

: 142632-71-1
r-2-Diphenylphosphinoyl-t-4,t-6-dimethyl-1,3-dioxane

: 130506-61-5
r-2-Diphenylphosphinoyl-c-4,c-6-dimethyl-1,3-dioxane

Guidance literature:: With benzenesulfonic acid; In benzene; for 2h; Heating;
DOI:10.1016/S0040-4020(01)92198-2

Reference yield:

: 142572-25-6,142632-73-3
2-N,N-Dimethylamino-cis-4,6-dimethyl-1,3-dioxane

: 130506-61-5
r-2-Diphenylphosphinoyl-c-4,c-6-dimethyl-1,3-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: 89.8 percent / diethyl ether

2: 66.4 percent / toluene / 3 h / Heating

In diethyl ether; toluene;
DOI:10.1016/S0040-4020(01)92198-2