3-[(2-Methoxyphenyl)methyl]oxolane-2,5-dione

Base Information

Chemical Name:3-[(2-Methoxyphenyl)methyl]oxolane-2,5-dione
CAS No.:32298-35-4
Molecular Formula:C₁₂H₁₂O₄
Molecular Weight:220.225
Hs Code.:
DSSTox Substance ID:DTXSID601226134

Synonyms:32298-35-4;DTXSID601226134;Dihydro-3-[(2-methoxyphenyl)methyl]-2,5-furandione

Suppliers and Price of 3-[(2-Methoxyphenyl)methyl]oxolane-2,5-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-[(2-Methoxyphenyl)methyl]oxolane-2,5-dione

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:220.07355886
Heavy Atom Count:16
Complexity:287

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=CC=C1CC2CC(=O)OC2=O

Technology Process of 3-[(2-Methoxyphenyl)methyl]oxolane-2,5-dione

There total 5 articles about 3-[(2-Methoxyphenyl)methyl]oxolane-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 32298-34-3
(2-methoxy benzyl) succinic acid

: 32298-35-4
(2-methoxy benzyl) succinic anhydride

Guidance literature:: With acetic anhydride; for 2h; Heating;
DOI:10.1080/00397919208020492

Reference yield:

: 2-(2-Methoxy-benzyl)-succinic acid diethyl ester

: 32298-35-4
(2-methoxy benzyl) succinic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1: 87.6 percent / H₂ / 10percent Pd/C / acetic acid

2: 88 percent / acetic anhydride / 2 h / Heating

With hydrogen; acetic anhydride; palladium on activated charcoal; In acetic acid;
DOI:10.1080/00397919208020492

Reference yield:

: 135-02-4
ortho-anisaldehyde

: 32298-35-4
(2-methoxy benzyl) succinic anhydride

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / Na / ethanol / 2 h / Heating

2: 87.6 percent / H₂ / 10percent Pd/C / acetic acid

3: 88 percent / acetic anhydride / 2 h / Heating

With hydrogen; sodium; acetic anhydride; palladium on activated charcoal; In ethanol; acetic acid;
DOI:10.1080/00397919208020492