Ethyl-N-cyclohexylbenzimidat

Base Information

• Chemical Name: Ethyl-N-cyclohexylbenzimidat
• CAS No.: 23604-74-2
• Molecular Formula: C₁₅H₂₁NO
• Molecular Weight: 231.338
• Mol file: 23604-74-2.mol

Synonyms:

Chemical Property of Ethyl-N-cyclohexylbenzimidat

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ethyl-N-cyclohexylbenzimidat

There total 3 articles about Ethyl-N-cyclohexylbenzimidat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

bromobenzene (108-86-1,52753-63-6) + Cyclohexyl isocyanide (931-53-3) + ethanol (64-17-5) → Ethyl-N-cyclohexylbenzimidat (23604-74-2) + N-cyclohexyl-2-cyclohexylimino-2-phenyl-acetimidic acid ethyl ester

Guidance literature:

With 1,1'-bis-(diphenylphosphino)ferrocene; sodium ethanolate; palladium dichloride; In 1,4-dioxane; at 98 ℃; for 15h; Further Variations:; Temperatures; Reagents; Solvents; time; Product distribution;

DOI:10.1039/b408673m

Reference yield:

N-benzoylcyclohexylamine (1759-68-8) + triethyloxonium fluoroborate (368-39-8) → Ethyl-N-cyclohexylbenzimidat (23604-74-2)

Guidance literature:

In dichloromethane; Heating;

Reference yield:

ethanol (64-17-5) + benzonitrile (100-47-0) + cyclohexene (110-83-8) → Ethyl-N-cyclohexylbenzimidat (23604-74-2)

Guidance literature:

Multistep reaction; (i) HF, (ii) /BRN= 1718733/, NH₃;

DOI:10.1021/jo00830a077

upstream raw materials:

N-benzoylcyclohexylamine

triethyloxonium fluoroborate

ethanol

benzonitrile

Refernces