OsClCHC(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2

Base Information

Chemical Name:OsClCHC(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2
CAS No.:349547-81-5
Molecular Formula:C₃₀H₅₄ClNOOsP₂
Molecular Weight:732.365
Hs Code.:

OsClCHC(C<sub>6</sub>H<sub>5</sub>)NC(CH<sub>3</sub>)2(CO)(P(C<sub>3</sub>H<sub>7</sub>)3)2

Synonyms:

Suppliers and Price of OsClCHC(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of OsClCHC(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2

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Technology Process of OsClCHC(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2

There total 1 articles about OsClCHC(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: OsClCHCH(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2⁽¹⁺⁾*CF₃SO₃^(1-)=OsClCHCH(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2(CF₃SO₃)

: 917-54-4
methyllithium

: 349547-81-5
OsClCHC(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2

Guidance literature:: In tetrahydrofuran; byproducts: LiCF3SO3, CH4; a suspn. of complex in THF was treated with a soln. of MeLi in diethyl ether, 5 min, (Ar); the solvent was evapd. to dryness, toluene was added, filtered, concd. to dryness, methanol was added, ppt. was washed with methanol and dried in vac.; elem. anal.;
DOI:10.1021/om010005k

Reference yield: 99.0%

: 349547-81-5
OsClCHC(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2

: 1333-74-0
hydrogen

: 349547-83-7
(CH₃)2CNCC₆H₅CH₂

: 183472-56-2
Os(H)2(H₂)(CO)(P(CH(CH₃)2)3)2

Guidance literature:: In benzene-d6; a slow stream of H2 was bubbled through a soln. of complex in benzene-d6, 5 h; detected by NMR spectra;
DOI:10.1021/om010005k

Reference yield: 81.0%

: 349547-81-5
OsClCHC(C₆H₅)NC(CH₃)2(CO)(P(C₃H₇)3)2

: 201230-82-2
carbon monoxide

: 349547-85-9
[Os((Z)-CH=C(Ph)N=C(CH₃)2)Cl(CO)2(PiPr₃)2]BF₄

Guidance literature:: In toluene; CO was bubbled through a soln. of complex in toluene for 15 min; the solvent was concd. to dryness, methanol was added, ppt. was washed with methanol and dried in vac.; elem. anal.;
DOI:10.1021/om010005k