[Fe₂(CO)6(CH₂S)2N-C₆H₁₁]

Base Information

Chemical Name:[Fe₂(CO)6(CH₂S)2N-C₆H₁₁]
CAS No.:950183-62-7
Molecular Formula:C₁₄H₁₅Fe₂NO₆S₂
Molecular Weight:469.102
Hs Code.:

[Fe<sub>2</sub>(CO)6(CH<sub>2</sub>S)2N-C<sub>6</sub>H<sub>11</sub>]

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Chemical Property of [Fe₂(CO)6(CH₂S)2N-C₆H₁₁]

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Technology Process of [Fe₂(CO)6(CH₂S)2N-C₆H₁₁]

There total 1 articles about [Fe₂(CO)6(CH₂S)2N-C₆H₁₁] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 14243-23-3
(μ-dithio)bis(tricarbonyliron)

: 108-91-8,157973-60-9
cyclohexylamine

: 950183-62-7
[Fe₂(CO)6(CH₂S)2N-C₆H₁₁]

Guidance literature:: With LiBEt₃H; F₃CCOOH; In tetrahydrofuran; under N2; a soln. of Fe2-contg. compd. in THF was cooled to -78°C; stirring for 30 min; B-contg. compd. was added dropwise; after 30 min,F3CCOOH was added; stirring for 1 h; cool soln. was added to a mixt. of paraformaldehyde and C6H11NH2 in THF; after stirring for 24 h the majority of the solvent was evapd. under vac.; the remaining soln. was filtered through silica gel; a red fraction was collected by elution with hexane; recrystn. from hexane; elem. anal.;
DOI:10.1039/b616236c