methyl 3--2-methylsulfonyldithiocinnamate

Base Information

Chemical Name:methyl 3--2-methylsulfonyldithiocinnamate
CAS No.:117236-66-5
Molecular Formula:C₁₄H₁₇NO₄S₃
Molecular Weight:359.491
Hs Code.:

methyl 3-<bis(methoxy)methyleneamino>-2-methylsulfonyldithiocinnamate

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Suppliers and Price of methyl 3--2-methylsulfonyldithiocinnamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3--2-methylsulfonyldithiocinnamate

Chemical Property:

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Technology Process of methyl 3--2-methylsulfonyldithiocinnamate

There total 3 articles about methyl 3--2-methylsulfonyldithiocinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 67-56-1
methanol

: 117236-65-4
2-methoxy-5-methylsulfonyl-4-phenyl-1,3-thiazine-6-thione

: 74-88-4
methyl iodide

: 117236-66-5
methyl 3--2-methylsulfonyldithiocinnamate

Guidance literature:: With triethylamine; for 2h;

Reference yield:

: 117235-95-7
5-methylsulfonyl-2-methylthio-4-phenyl-1,3-thiazine-6-thione

: 117236-66-5
methyl 3--2-methylsulfonyldithiocinnamate

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / Et₃N / tetrahydrofuran / 24 h

2: 31 percent / Et₃N / 2 h

With triethylamine; In tetrahydrofuran;

Reference yield:

: 69143-56-2
5-methylsulphonyl-4-phenyl-1,3-thiazine-2,6(3H)-dithione

: 117236-66-5
methyl 3--2-methylsulfonyldithiocinnamate

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / tetrahydrofuran

2: 27 percent / Et₃N / tetrahydrofuran / 24 h

3: 31 percent / Et₃N / 2 h

With triethylamine; In tetrahydrofuran;