di-(-)-menthyl diethylmalonate

Base Information

Chemical Name:di-(-)-menthyl diethylmalonate
CAS No.:528846-20-0
Molecular Formula:C₂₇H₄₈O₄
Molecular Weight:436.676
Hs Code.:

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Suppliers and Price of di-(-)-menthyl diethylmalonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-(-)-menthyl diethylmalonate

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Technology Process of di-(-)-menthyl diethylmalonate

There total 4 articles about di-(-)-menthyl diethylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 73636-64-3
di-l-menthyl malonate

: 75-03-6
ethyl iodide

: 528846-20-0
di-(-)-menthyl diethylmalonate

Guidance literature:: di-l-menthyl malonate; With sodium ethanolate; In tetrahydrofuran; for 1h;

ethyl iodide; In tetrahydrofuran; for 3h;
DOI:10.1080/10242430215697

Reference yield:

: 2216-51-5
(-)-menthol

: 528846-20-0
di-(-)-menthyl diethylmalonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 66 percent / triethylamine / CCl₃F / 1 h

2.1: sodium ethoxide / tetrahydrofuran / 1 h

2.2: 70 percent / tetrahydrofuran / 3 h

With sodium ethanolate; triethylamine; In tetrahydrofuran; trichlorofluoromethane;
DOI:10.1080/10242430215697