(+/-)-sym-dichloro[3-[1-(diphenylphosphino)ethyl]-2,7-dimethyl-4-naphthalenyl-P]-3',4'-dimethyl-1'-phenylphospholepalladium(II)*dichloromethane

Base Information

Chemical Name:(+/-)-sym-dichloro[3-[1-(diphenylphosphino)ethyl]-2,7-dimethyl-4-naphthalenyl-P]-3',4'-dimethyl-1'-phenylphospholepalladium(II)*dichloromethane
CAS No.:1178888-24-8
Molecular Formula:CH₂Cl₂*C₃₈H₃₈Cl₂P₂Pd
Molecular Weight:818.926
Hs Code.:

(+/-)-sym-dichloro[3-[1-(diphenylphosphino)ethyl]-2,7-dimethyl-4-naphthalenyl-P]-3',4'-dimethyl-1'-phenylphospholepalladium(II)*dichloromethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-sym-dichloro[3-[1-(diphenylphosphino)ethyl]-2,7-dimethyl-4-naphthalenyl-P]-3',4'-dimethyl-1'-phenylphospholepalladium(II)*dichloromethane

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Technology Process of (+/-)-sym-dichloro[3-[1-(diphenylphosphino)ethyl]-2,7-dimethyl-4-naphthalenyl-P]-3',4'-dimethyl-1'-phenylphospholepalladium(II)*dichloromethane

There total 1 articles about (+/-)-sym-dichloro[3-[1-(diphenylphosphino)ethyl]-2,7-dimethyl-4-naphthalenyl-P]-3',4'-dimethyl-1'-phenylphospholepalladium(II)*dichloromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.2%

: 7647-01-0,15364-23-5
hydrogenchloride

: 75-09-2
dichloromethane

: 1178887-97-2,1179901-33-7,1179901-34-8,1179901-36-0
(+/-)-chloro[3-[1-(diphenylphosphino)ethyl]-2,7-dimethyl-4-naphthalenyl-C,P]-3',4'-dimethyl-1'-phenylphospholepalladium(II)

: 1178888-24-8
(+/-)-sym-dichloro[3-[1-(diphenylphosphino)ethyl]-2,7-dimethyl-4-naphthalenyl-P]-3',4'-dimethyl-1'-phenylphospholepalladium(II)*dichloromethane

Guidance literature:: In hydrogenchloride; acetone; addn. of concd. aq. HCl to acetone soln. of palladium compd., stirring for 1 h at room temp.; washing with water, separating organic layer, drying over MgSO4, evapn.,chromy. (silica gel, CH2Cl2/acetone (1:1)), elem. anal.;
DOI:10.1021/om900423f