(6-methoxyquinolin-8-yl)(phenyl)methanone

Base Information

Chemical Name:(6-methoxyquinolin-8-yl)(phenyl)methanone
CAS No.:1438559-19-3
Molecular Formula:C₁₇H₁₃NO₂
Molecular Weight:263.296
Hs Code.:

Synonyms:

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Chemical Property of (6-methoxyquinolin-8-yl)(phenyl)methanone

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Technology Process of (6-methoxyquinolin-8-yl)(phenyl)methanone

There total 4 articles about (6-methoxyquinolin-8-yl)(phenyl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-71-1
3-Hydroxyacetophenone

: 1438559-19-3
(6-methoxyquinolin-8-yl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid; potassium nitrate / 1.17 h / 60 °C / Inert atmosphere

2: potassium carbonate / acetone / 20 °C / Inert atmosphere

3: tin(ll) chloride / ethanol / 1 h / Reflux; Inert atmosphere

4: sodium meta-nitrobenzenesulfonic acid; ferrous(II) sulfate heptahydrate / methanesulfonic acid / 120 °C / Inert atmosphere

5: potassium carbonate; Wilkinson’s catalyst; copper(l) iodide / 5,5-dimethyl-1,3-cyclohexadiene / 18 h / 130 °C

With ferrous(II) sulfate heptahydrate; copper(l) iodide; Wilkinson’s catalyst; sodium meta-nitrobenzenesulfonic acid; potassium carbonate; acetic acid; potassium nitrate; tin(ll) chloride; In methanesulfonic acid; 5,5-dimethyl-1,3-cyclohexadiene; ethanol; acetone;
DOI:10.1002/anie.201206693

Reference yield:

: 42887-67-2
1-(5-methoxy-2-nitrophenyl)ethanone

: 1438559-19-3
(6-methoxyquinolin-8-yl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 3 steps

1: tin(ll) chloride / ethanol / 1 h / Reflux; Inert atmosphere

2: sodium meta-nitrobenzenesulfonic acid; ferrous(II) sulfate heptahydrate / methanesulfonic acid / 120 °C / Inert atmosphere

3: potassium carbonate; Wilkinson’s catalyst; copper(l) iodide / 5,5-dimethyl-1,3-cyclohexadiene / 18 h / 130 °C

With ferrous(II) sulfate heptahydrate; copper(l) iodide; Wilkinson’s catalyst; sodium meta-nitrobenzenesulfonic acid; potassium carbonate; tin(ll) chloride; In methanesulfonic acid; 5,5-dimethyl-1,3-cyclohexadiene; ethanol;
DOI:10.1002/anie.201206693

Reference yield:

: 23042-77-5
1-(2-amino-5-methoxy-phenyl)-ethanone

: 1438559-19-3
(6-methoxyquinolin-8-yl)(phenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: sodium meta-nitrobenzenesulfonic acid; ferrous(II) sulfate heptahydrate / methanesulfonic acid / 120 °C / Inert atmosphere

2: potassium carbonate; Wilkinson’s catalyst; copper(l) iodide / 5,5-dimethyl-1,3-cyclohexadiene / 18 h / 130 °C

With ferrous(II) sulfate heptahydrate; copper(l) iodide; Wilkinson’s catalyst; sodium meta-nitrobenzenesulfonic acid; potassium carbonate; In methanesulfonic acid; 5,5-dimethyl-1,3-cyclohexadiene;
DOI:10.1002/anie.201206693