2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE

Base Information

Chemical Name:2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE
CAS No.:337921-66-1
Molecular Formula:C₂₀H₁₄O₂
Molecular Weight:286.33
Hs Code.:
Mol file:337921-66-1.mol

Synonyms:

Suppliers and Price of 2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2-(2-Furylmethylene)-3-phenyl-1-indanone
10mg
$ 146.00

Matrix Scientific
2-(2-Furylmethylene)-3-phenyl-1-indanone
5mg
$ 105.00

Matrix Scientific
2-(2-Furylmethylene)-3-phenyl-1-indanone
1mg
$ 90.00

American Custom Chemicals Corporation
2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE 95.00%
5G
$ 1928.08

American Custom Chemicals Corporation
2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE 95.00%
1MG
$ 647.61

Total 2 raw suppliers

Chemical Property of 2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

2-(2-Furylmethylene)-3-phenyl-1-indanone ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE

There total 8 articles about 2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1666-17-7
benzaldehyde p-toluenesulfonylhydrazone

: 1258504-75-4
C₁₃H₉IO₂

: 337921-66-1
(E)-2-(furan-2-ylmethylene)-3-phenyl-2,3-dihydro-1H-inden-1-one

Guidance literature:: With palladium diacetate; potassium carbonate; triphenylphosphine; In tetrahydrofuran; water; at 60 ℃; for 3h; stereoselective reaction;
DOI:10.1021/acs.orglett.5b02803

Reference yield:

: 300657-41-4
(E)-1-(2-bromophenyl)-3-phenylprop-2-en-1-one

: 337921-66-1
C₂₀H₁₄O₂

Guidance literature:: Multi-step reaction with 2 steps

1: water; (4S)-(+)-phenyl-α-[(4S)-phenyloxazolidin-2-ylidene]-2-oxazoline-2-acetonitrile; nickel(II) bromide dimethoxyethane; manganese; lithium carbonate / N,N-dimethyl-formamide; tetrahydrofuran / 24 h / 80 °C / Inert atmosphere; Glovebox; Schlenk technique

2: N,N-dimethyl-formamide; tetrahydrofuran / 24 h / 90 °C / Inert atmosphere; Glovebox; Schlenk technique

With nickel(II) bromide dimethoxyethane; manganese; (4S)-(+)-phenyl-α-[(4S)-phenyloxazolidin-2-ylidene]-2-oxazoline-2-acetonitrile; water; lithium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide; 1: |Heck Reaction;
DOI:10.1021/acs.orglett.9b02130

Reference yield:

: 551-93-9
2-aminoacetophenone

: 337921-66-1
(E)-2-(furan-2-ylmethylene)-3-phenyl-2,3-dihydro-1H-inden-1-one

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid; sodium nitrite; potassium iodide / water; acetonitrile / 0 - 20 °C

2: sodium hydroxide / ethanol; water / 0 - 20 °C

3: palladium diacetate; triphenylphosphine; potassium carbonate / tetrahydrofuran; water / 3 h / 60 °C

With palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; potassium iodide; sodium hydroxide; sodium nitrite; In tetrahydrofuran; ethanol; water; acetonitrile;
DOI:10.1021/acs.orglett.5b02803