Technology Process of 2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE
There total 8 articles about 2-(2-FURYLMETHYLENE)-3-PHENYL-1-INDANONE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium diacetate; potassium carbonate; triphenylphosphine;
In
tetrahydrofuran; water;
at 60 ℃;
for 3h;
stereoselective reaction;
DOI:10.1021/acs.orglett.5b02803
- Guidance literature:
-
Multi-step reaction with 2 steps
1: water; (4S)-(+)-phenyl-α-[(4S)-phenyloxazolidin-2-ylidene]-2-oxazoline-2-acetonitrile; nickel(II) bromide dimethoxyethane; manganese; lithium carbonate / N,N-dimethyl-formamide; tetrahydrofuran / 24 h / 80 °C / Inert atmosphere; Glovebox; Schlenk technique
2: N,N-dimethyl-formamide; tetrahydrofuran / 24 h / 90 °C / Inert atmosphere; Glovebox; Schlenk technique
With
nickel(II) bromide dimethoxyethane; manganese; (4S)-(+)-phenyl-α-[(4S)-phenyloxazolidin-2-ylidene]-2-oxazoline-2-acetonitrile; water; lithium carbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
1: |Heck Reaction;
DOI:10.1021/acs.orglett.9b02130
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid; sodium nitrite; potassium iodide / water; acetonitrile / 0 - 20 °C
2: sodium hydroxide / ethanol; water / 0 - 20 °C
3: palladium diacetate; triphenylphosphine; potassium carbonate / tetrahydrofuran; water / 3 h / 60 °C
With
palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; potassium iodide; sodium hydroxide; sodium nitrite;
In
tetrahydrofuran; ethanol; water; acetonitrile;
DOI:10.1021/acs.orglett.5b02803
