S,S-dimethyl 5-benzyl-1,3,4-thiadiazol-2-yldithioimidocarbonate

Base Information

• Chemical Name: S,S-dimethyl 5-benzyl-1,3,4-thiadiazol-2-yldithioimidocarbonate
• CAS No.: 1001440-83-0
• Molecular Formula: C₁₂H₁₃N₃S₃
• Molecular Weight: 295.453
• Mol file: 1001440-83-0.mol

Synonyms:

Chemical Property of S,S-dimethyl 5-benzyl-1,3,4-thiadiazol-2-yldithioimidocarbonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S,S-dimethyl 5-benzyl-1,3,4-thiadiazol-2-yldithioimidocarbonate

There total 1 articles about S,S-dimethyl 5-benzyl-1,3,4-thiadiazol-2-yldithioimidocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + 5-benzyl-[1,3,4]thiadiazol-2-ylamine (16502-08-2) + methyl iodide (74-88-4) → S,S-dimethyl 5-benzyl-1,3,4-thiadiazol-2-yldithioimidocarbonate (1001440-83-0)

Guidance literature:

carbon disulfide; 5-benzyl-[1,3,4]thiadiazol-2-ylamine; With sodium hydroxide; In N,N-dimethyl-formamide; at 0 - 5 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h; Further stages.;

DOI:10.1080/10426500601088721

Reference yield: 72.0%

S,S-dimethyl 5-benzyl-1,3,4-thiadiazol-2-yldithioimidocarbonate (1001440-83-0) + 1,2-diamino-benzene (95-54-5) → N-(5-benzyl-1,3,4-thiadiazol-2-yl)-1H-benzimidazol-2-amine

Guidance literature:

In N,N-dimethyl-formamide; at 120 ℃; for 8h;

DOI:10.1080/10426500601088721

Reference yield: 69.0%

S,S-dimethyl 5-benzyl-1,3,4-thiadiazol-2-yldithioimidocarbonate (1001440-83-0) + 2-amino-phenol (95-55-6) → N-(5-benzyl-1,3,4-thiadiazol-2-yl)-1,3-benzoxazol-2-amine

Guidance literature:

In N,N-dimethyl-formamide; at 120 ℃; for 8h;

DOI:10.1080/10426500601088721

upstream raw materials:

carbon disulfide

5-benzyl-[1,3,4]thiadiazol-2-ylamine

methyl iodide