Technology Process of C15H12ClNO3S
There total 8 articles about C15H12ClNO3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trichlorophosphate / 20 - 150 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C
2.2: 2 h / 0 - 20 °C
3.1: sodium hydroxide / water; methanol / 2 h / 0 - 50 °C
3.2: 0 °C / pH 2
4.1: thionyl chloride / 20 °C / Inert atmosphere
With
thionyl chloride; potassium carbonate; sodium hydroxide; trichlorophosphate;
In
methanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: tetrabutylammomium bromide; sodium sulfite / water; methanol / 3 h / 20 - 100 °C
2.1: hydrogen; palladium 10% on activated carbon / methanol / 12 h / 3102.97 Torr / Inert atmosphere
3.1: trichlorophosphate / 20 - 150 °C
4.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C
4.2: 2 h / 0 - 20 °C
5.1: sodium hydroxide / water; methanol / 2 h / 0 - 50 °C
5.2: 0 °C / pH 2
6.1: thionyl chloride / 20 °C / Inert atmosphere
With
thionyl chloride; palladium 10% on activated carbon; tetrabutylammomium bromide; hydrogen; potassium carbonate; sodium hydroxide; sodium sulfite; trichlorophosphate;
In
methanol; water; N,N-dimethyl-formamide;
- Guidance literature:
-
With
thionyl chloride;
at 20 ℃;
Inert atmosphere;
