4-[(E)-(4-Methoxyphenyl)diazenyl]-1-methylpyridin-1-ium iodide

Base Information

Chemical Name:4-[(E)-(4-Methoxyphenyl)diazenyl]-1-methylpyridin-1-ium iodide
CAS No.:111317-33-0
Molecular Formula:C13H14N3O.I
Molecular Weight:355.178
Hs Code.:
DSSTox Substance ID:DTXSID00579645

Synonyms:111317-33-0;DTXSID00579645;4-[(E)-(4-Methoxyphenyl)diazenyl]-1-methylpyridin-1-ium iodide

Suppliers and Price of 4-[(E)-(4-Methoxyphenyl)diazenyl]-1-methylpyridin-1-ium iodide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[(E)-(4-Methoxyphenyl)diazenyl]-1-methylpyridin-1-ium iodide

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:355.01816
Heavy Atom Count:18
Complexity:241

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[N+]1=CC=C(C=C1)N=NC2=CC=C(C=C2)OC.[I-]

Technology Process of 4-[(E)-(4-Methoxyphenyl)diazenyl]-1-methylpyridin-1-ium iodide

There total 2 articles about 4-[(E)-(4-Methoxyphenyl)diazenyl]-1-methylpyridin-1-ium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 20815-67-2
4-(p'-methoxyphenylazo)pyridine

: 74-88-4
methyl iodide

: 111317-33-0
4-(p-methoxyphenylazo)pyridinium methiodide

Guidance literature:: In methanol; at 74 ℃; for 8h;
DOI:10.3987/R-1987-02-0313

Reference yield:

: 20815-66-1
4-(2-(pyridin-4-yl)diazenyl)phenol

: 111317-33-0
4-(p-methoxyphenylazo)pyridinium methiodide

Guidance literature:: Multi-step reaction with 2 steps

1: 0.1 M methanolic H₂SO₄ / 4 h / Heating

2: 21 percent / methanol / 8 h / 74 °C

With sulfuric acid; In methanol;
DOI:10.3987/R-1987-02-0313