(-)-(3R)-methyl-4-penten-1-ol

Base Information Edit

Chemical Name:(-)-(3R)-methyl-4-penten-1-ol
CAS No.:75420-44-9
Molecular Formula:C₆H₁₂O
Molecular Weight:100.161
Hs Code.:
Mol file:75420-44-9.mol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-(3R)-methyl-4-penten-1-ol Edit

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Technology Process of (-)-(3R)-methyl-4-penten-1-ol

There total 12 articles about (-)-(3R)-methyl-4-penten-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: (S)-3-[(R)-3-methylpent-4-enoyl]-4-phenyloxazolidin-2-one

: 75420-44-9,54702-04-4
(-)-(3R)-methyl-4-penten-1-ol

Guidance literature:: With lithium tetrahydridoborate; In tetrahydrofuran; diethyl ether; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/acs.orglett.2c00349

Reference yield:

: 10281-56-8
(R)-3,7-dimethyl-1,6-octadiene

: 75420-44-9,54702-04-4
(-)-(3R)-methyl-4-penten-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1: 40percent peracetic acid, sodium acetate / CH₂Cl₂; H₂O / 2 h / 20 °C

2: LiClO₄ / petroleum ether / 5 h / Heating

3: 1) potassium t-butoxide, oxygen, 2) LiAlH₄ / 1) glyme, 90 min, 2) ether, reflux, 8 h

With peracetic acid; lithium aluminium tetrahydride; potassium tert-butylate; oxygen; sodium acetate; lithium perchlorate; In dichloromethane; water; Petroleum ether;
DOI:10.1002/hlca.19810640515