3,4,5-Trimethoxy-benzoic acid 2-{4-[3-(3,4-dichloro-phenyl)-3-hydroxy-pentyl]-piperazin-1-yl}-ethyl ester; compound with (Z)-but-2-enedioic acid

Base Information

Chemical Name:3,4,5-Trimethoxy-benzoic acid 2-{4-[3-(3,4-dichloro-phenyl)-3-hydroxy-pentyl]-piperazin-1-yl}-ethyl ester; compound with (Z)-but-2-enedioic acid
CAS No.:113699-88-0
Molecular Formula:2C₄H₄O₄*C₂₇H₃₆Cl₂N₂O₆
Molecular Weight:787.645
Hs Code.:

3,4,5-Trimethoxy-benzoic acid 2-{4-[3-(3,4-dichloro-phenyl)-3-hydroxy-pentyl]-piperazin-1-yl}-ethyl ester; compound with (Z)-but-2-enedioic acid

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Chemical Property of 3,4,5-Trimethoxy-benzoic acid 2-{4-[3-(3,4-dichloro-phenyl)-3-hydroxy-pentyl]-piperazin-1-yl}-ethyl ester; compound with (Z)-but-2-enedioic acid

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Technology Process of 3,4,5-Trimethoxy-benzoic acid 2-{4-[3-(3,4-dichloro-phenyl)-3-hydroxy-pentyl]-piperazin-1-yl}-ethyl ester; compound with (Z)-but-2-enedioic acid

There total 3 articles about 3,4,5-Trimethoxy-benzoic acid 2-{4-[3-(3,4-dichloro-phenyl)-3-hydroxy-pentyl]-piperazin-1-yl}-ethyl ester; compound with (Z)-but-2-enedioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 113699-84-6
1-<3-(3,4-dichlorophenyl)-3-hydroxypentyl>-4-(2-hydroxyethyl)piperazine dihydrochloride

: 118-41-2
Eudesmic acid

: 113699-88-0
3,4,5-Trimethoxy-benzoic acid 2-{4-[3-(3,4-dichloro-phenyl)-3-hydroxy-pentyl]-piperazin-1-yl}-ethyl ester; compound with (Z)-but-2-enedioic acid

Guidance literature:: With triethylamine; In dichloromethane; for 1.5h;
DOI:10.1248/cpb.35.2782

Reference yield:

: 103-76-4
1-(2-hydroxyethyl)piperazine

: 113699-88-0
3,4,5-Trimethoxy-benzoic acid 2-{4-[3-(3,4-dichloro-phenyl)-3-hydroxy-pentyl]-piperazin-1-yl}-ethyl ester; compound with (Z)-but-2-enedioic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 14 percent / triethylamine (Et₃N) / xylene / 4.5 h / Heating

2: 16 percent / triethylamine (Et₃N) / CH₂Cl₂ / 1.5 h

With triethylamine; In dichloromethane; xylene;
DOI:10.1248/cpb.35.2782

Reference yield:

: 107049-58-1
1-Chloro-3-(3,4-dichloro-phenyl)-pentan-3-ol

: 113699-88-0
3,4,5-Trimethoxy-benzoic acid 2-{4-[3-(3,4-dichloro-phenyl)-3-hydroxy-pentyl]-piperazin-1-yl}-ethyl ester; compound with (Z)-but-2-enedioic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 14 percent / triethylamine (Et₃N) / xylene / 4.5 h / Heating

2: 16 percent / triethylamine (Et₃N) / CH₂Cl₂ / 1.5 h

With triethylamine; In dichloromethane; xylene;
DOI:10.1248/cpb.35.2782