cis-bis(triphenylphosphine)platinum(II) ethane-1,2-dithiolate

Base Information

Chemical Name:cis-bis(triphenylphosphine)platinum(II) ethane-1,2-dithiolate
CAS No.:56213-51-5
Molecular Formula:C₃₈H₃₄P₂PtS₂
Molecular Weight:811.847
Hs Code.:

Synonyms:

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Chemical Property of cis-bis(triphenylphosphine)platinum(II) ethane-1,2-dithiolate

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Technology Process of cis-bis(triphenylphosphine)platinum(II) ethane-1,2-dithiolate

There total 1 articles about cis-bis(triphenylphosphine)platinum(II) ethane-1,2-dithiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 442848-88-6
[(triphenylphosphine)2Pt(μ-S(CH2)2S)Rh(carbonyl)2]ClO4

: 6737-42-4
1,3-bis-(diphenylphosphino)propane

: [(PPh₂(CH₂)3PPh₂)2Rh(carbonyl)]⁽¹⁺⁾

: 56213-51-5
cis-bis(triphenylphosphine)platinum(II) ethane-1,2-dithiolate

Guidance literature:: In chloroform-d1; under N2; a soln. of PtRh bimetallic complex was treated with the phosphine; not isolated, monitored by NMR;
DOI:10.1021/om020042r

Reference yield: 87.0%

: 59420-05-2
bis(cyclooctadiene)rhodium(I) perchlorate

: 56213-51-5
cis-bis(triphenylphosphine)platinum(II) ethane-1,2-dithiolate

: 200009-04-7
[(PPh3)2Pt(μ-ethane-1,2-dithiolate)Rh(1,5-cyclooctadiene)]ClO4

Guidance literature:: In dichloromethane; byproducts: COD; N2-atmosphere; stirring stoich. amts. at room temp. for 30 min; concn., crystn. on addn. or vapor diffusion of hexane; elem. anal.;
DOI:10.1021/ic970557o

Reference yield: 80.0%

: 14104-20-2
silver tetrafluoroborate

: μ2-dichlorobis(chloro(cyclopentadienyl)rhodium)

: 56213-51-5
cis-bis(triphenylphosphine)platinum(II) ethane-1,2-dithiolate

: 500199-76-8
[(PPh3)2Pt(μ-S(CH2)2S)RhCl(η5-C5H5)]BF4

Guidance literature:: In tetrahydrofuran; byproducts: AgCl; under N2; AgBF4 (0.1826 mmol) was added to a suspn. of Rh-contg. compd. (0.0913 mmol) in anhyd. and deoxigenated THF; stirring for 5 min at roomtemp.; then Pt-contg. compd. (0.1826 mmol) was added; AgCl was removed by filtration; the filtrate was concd. and the ppt. wasobtained by C6H14 addn.; the solid was filtrated, washed with C6H14 and dried under vac.; elem. anal.;
DOI:10.1016/S0022-328X(02)01925-3