(4E)-N-Benzyl-1,2,5-trimethylpiperidin-4-imine

Base Information

• Chemical Name: (4E)-N-Benzyl-1,2,5-trimethylpiperidin-4-imine
• CAS No.: 113556-33-5
• Molecular Formula: C15H22N2
• Molecular Weight: 230.353
• DSSTox Substance ID: DTXSID80549169
• Nikkaji Number: J400.735B
• Mol file: 113556-33-5.mol

Synonyms:113556-33-5;(4E)-N-Benzyl-1,2,5-trimethylpiperidin-4-imine;DTXSID80549169

Chemical Property of (4E)-N-Benzyl-1,2,5-trimethylpiperidin-4-imine

Chemical Property:

• XLogP3: 2.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 230.178298710
• Heavy Atom Count: 17
• Complexity: 266

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1CC(=NCC2=CC=CC=C2)C(CN1C)C

Technology Process of (4E)-N-Benzyl-1,2,5-trimethylpiperidin-4-imine

There total 1 articles about (4E)-N-Benzyl-1,2,5-trimethylpiperidin-4-imine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.5%

1,2,5-trimethyl-4-piperidone (7516-33-8) + benzylamine (100-46-9) → N-(1-methyl-2,5-dimethyl-4-piperidylidene)benzylamine (113556-33-5)

Guidance literature:

With zinc(II) chloride; In toluene; Heating; catalytic amount of acetic acid, benzene;

DOI:10.1007/BF00475650

Reference yield: 75.0%

N-(1-methyl-2,5-dimethyl-4-piperidylidene)benzylamine (113556-33-5) + allylmagnesium bromide (1730-25-2) → 1-methyl-2,5-dimethyl-4-allyl-4-N-benzylaminopiperidine (129115-32-8)

Guidance literature:

With dibenzo-18-crown-6; In diethyl ether; for 5h; Heating;

DOI:10.1007/BF00481521

Reference yield: 54.0%

propionyl chloride (79-03-8) + 1,2,5-trimethyl-4-N-benzyliminopiperidine (113556-33-5) → N-Benzyl-N-(1,3,6-trimethyl-1,2,3,6-tetrahydro-pyridin-4-yl)-propionamide (135901-35-8)

Guidance literature:

With triethylamine; In diethyl ether; at 5 - 25 ℃; for 15h;

DOI:10.1007/BF00772137

upstream raw materials:

1,2,5-trimethyl-4-piperidone

benzylamine

Downstream raw materials:

N-benzyl-N-(1,2,5-trimethyl-4-piperidinyl)amine

1,2,5-trimethyl-4-phenyl-4-N-benzylaminopiperidine

1,2,5-trimethyl-4-propargyl-4-N-benzylaminopiperidine

1-methyl-2,5-dimethyl-4-allyl-4-N-benzylaminopiperidine

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