Technology Process of Cy-PSe
There total 4 articles about Cy-PSe which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium tetrahydroborate / ethanol / Inert atmosphere; Cooling with ice
1.2: 4 h / Inert atmosphere; Reflux
2.1: hydrogen / ethanol / 10 h / 85 °C / 30003 Torr / Autoclave
3.1: N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere
With
sodium tetrahydroborate; hydrogen;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja202582x
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: selenium / diethyl ether / 0.5 h / Reflux
1.2: Cooling with ice
2.1: sodium tetrahydroborate / ethanol / Inert atmosphere; Cooling with ice
2.2: 4 h / Inert atmosphere; Reflux
3.1: hydrogen / ethanol / 10 h / 85 °C / 30003 Torr / Autoclave
4.1: N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere
With
selenium; sodium tetrahydroborate; hydrogen;
In
diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja202582x
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium tetrahydroborate / ethanol / Inert atmosphere; Cooling with ice
1.2: 4 h / Inert atmosphere; Reflux
2.1: hydrogen / ethanol / 10 h / 85 °C / 30003 Torr / Autoclave
3.1: N,N-dimethyl-formamide / 24 h / 90 °C / Inert atmosphere
With
sodium tetrahydroborate; hydrogen;
In
ethanol; N,N-dimethyl-formamide;
DOI:10.1021/ja202582x
