Technology Process of 2-(benzyloxy)-9-methylacridine
There total 3 articles about 2-(benzyloxy)-9-methylacridine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butoxide; ruphos;
In
1,4-dioxane; water;
at 110 ℃;
for 12h;
regioselective reaction;
Microwave irradiation;
Inert atmosphere;
DOI:10.1002/ejoc.201201070
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / methanol / 6 h / 60 °C / Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); ruphos; lithium tert-butoxide / water; 1,4-dioxane / 12 h / 110 °C / Microwave irradiation; Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); toluene-4-sulfonic acid; lithium tert-butoxide; ruphos;
In
1,4-dioxane; methanol; water;
DOI:10.1002/ejoc.201201070
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); ruphos; lithium tert-butoxide / water; 1,4-dioxane / 12 h / 110 °C / Microwave irradiation; Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; lithium tert-butoxide; ruphos;
In
1,4-dioxane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201201070
