dichlorobis(α-benzyl oximato)ruthenium(III)

Base Information

Chemical Name:dichlorobis(α-benzyl oximato)ruthenium(III)
CAS No.:75400-19-0
Molecular Formula:C₂₈H₂₁Cl₂N₂O₄Ru
Molecular Weight:621.462
Hs Code.:

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Chemical Property of dichlorobis(α-benzyl oximato)ruthenium(III)

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Technology Process of dichlorobis(α-benzyl oximato)ruthenium(III)

There total 1 articles about dichlorobis(α-benzyl oximato)ruthenium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 14898-67-0
ruthenium(III) chloride trihydrate

: 574-15-2,574-16-3,14090-77-8,5351-34-8
benzilmonoxime

: 75400-19-0
dichlorobis(α-benzyl oximato)ruthenium(III)

Guidance literature:: In ethanol; α-benzyl oxime added to stirred soln. RuCl3*3H2O in abs. ethanol,mixt. warmed to 50°C and stirred for 2 h, than cooled to 0°C; ppt. filtered and washed with water and ethanol, crystals dried in vacuo over P4O10 and recrystd. from dichloromethane-diethyl ether; elem. anal.;

Reference yield: 80.0%

: 544-16-1
n-Butyl nitrite

: 75400-19-0
dichlorobis(α-benzyl oximato)ruthenium(III)

: 174094-71-4
RuC₂₈H₂₀N₃O₅Cl

Guidance literature:: In methanol; stirring (298 K, 1 h), cooling; filtration, soln. evapn. (red. pressure), pptn., washing (ether), redissoln. (methanol-water), soln. evapn., pptn., drying (vac.); IR monitoringat 1900 cm**-1, elem. anal.;

Reference yield: 70.0%

: 75400-19-0
dichlorobis(α-benzyl oximato)ruthenium(III)

: 7632-00-0
sodium nitrite

: 174094-71-4
RuC₂₈H₂₀N₃O₅Cl

Guidance literature:: With HCl; In methanol; trituration (323 K, 2 h), extn. (CHCl3); soln. evapn. (red. pressure), pptn., washing (ether), redissoln. (methanol-water), soln. evapn., pptn., drying (vac.); IR monitoring at 1900 cm**-1, elem. anal.;