Benzenemethanamine, N-cyclohexyl-a-methyl-

Base Information

• Chemical Name: Benzenemethanamine, N-cyclohexyl-a-methyl-
• CAS No.: 116692-81-0
• Molecular Formula: C14H21N
• Molecular Weight: 203.327
• Mol file: 116692-81-0.mol

Synonyms:

Chemical Property of Benzenemethanamine, N-cyclohexyl-a-methyl-

Chemical Property:

Purity/Quality:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanamine, N-cyclohexyl-a-methyl-

There total 16 articles about Benzenemethanamine, N-cyclohexyl-a-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-(1-phenylethylidene)cyclohexylamine (67888-71-5,1562-62-5) → N-(1-phenylethyl)cyclohexanamine (116692-81-0)

Guidance literature:

With zinc(II) tetrahydroborate; silica gel; In tetrahydrofuran; for 12h; Ambient temperature;

DOI:10.1021/jo961736a

Reference yield: 78.0%

→ N-(1-phenylethyl)cyclohexanamine (116692-81-0)

Guidance literature:

With C₂₅H₂₈ClIrN₂O₃; hydrogen; In 2,2,2-trifluoroethanol; at 75 ℃; for 1h; under 15001.5 Torr;

Reference yield: 71.0%

N-(1-phenylethylidene)cycloexanamine (731797-80-1) → N-(1-phenylethyl)cyclohexanamine (116692-81-0)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 18h;

DOI:10.1039/c9cc02900a

upstream raw materials:

N-(1-phenylethylidene)cyclohexylamine

N-(1-phenylethylidene)cycloexanamine

cyclohexylamine

acetophenone

Downstream raw materials:

cyclohexyl-(1-phenyl-ethyl)-carbamic acid-(2-piperidino-ethyl ester)

C₁₄H₂₁N*ClH

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