3-(4-chloro-2-methylphenyl)-1,1-dimethylthiourea

Base Information

Chemical Name:3-(4-chloro-2-methylphenyl)-1,1-dimethylthiourea
CAS No.:14501-88-3
Molecular Formula:C₁₀H₁₃ClN₂S
Molecular Weight:228.746
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-chloro-2-methylphenyl)-1,1-dimethylthiourea

Chemical Property:

Vapor Pressure:0.00136mmHg at 25°C

Purity/Quality:

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Technology Process of 3-(4-chloro-2-methylphenyl)-1,1-dimethylthiourea

There total 5 articles about 3-(4-chloro-2-methylphenyl)-1,1-dimethylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 23165-53-9
4-chloro-2-methylphenyl isothiocyanate

: 124-40-3
dimethyl amine

: 28217-97-2,14501-88-3
N-(4-chloro-2-methylphenyl)-N',N' dimethyl thiourea

Guidance literature:: In water; at 80 ℃; for 5h;
DOI:10.1002/anie.201710186

Reference yield: 93.0%

: 67-66-3,8013-54-5
chloroform

: 124-40-3
dimethyl amine

: 95-69-2
4-chloro-2-methylbenzeneamine

: 28217-97-2,14501-88-3
N-(4-chloro-2-methylphenyl)-N',N' dimethyl thiourea

Guidance literature:: chloroform; 4-chloro-2-methylbenzeneamine; With potassium hydroxide; In 1,4-dioxane; tert-butyl alcohol; at 55 ℃; for 4h;

dimethyl amine; With sulfur; potassium tert-butylate; In 1,4-dioxane; water; tert-butyl alcohol; at 55 ℃; for 12h;
DOI:10.1021/acs.orglett.7b00819

Reference yield: 63.0%

: 124-40-3
dimethyl amine

: (2-bromo-2,2-difluoro-acetyl)oxysodium

: 95-69-2
4-chloro-2-methylbenzeneamine

: 28217-97-2,14501-88-3
N-(4-chloro-2-methylphenyl)-N',N' dimethyl thiourea

Guidance literature:: sodium 2-bromo-2,2-difluoro-acetate; 4-chloro-2-methylbenzeneamine; With sulfur; potassium phosphate; copper(l) iodide; In acetonitrile; at 100 ℃; for 12h; Schlenk technique;

dimethyl amine; In tetrahydrofuran; acetonitrile; at 80 ℃; for 6h; Schlenk technique;
DOI:10.1039/c8cc09190k