butyl phenylphosphorazidate

Base Information

• Chemical Name: butyl phenylphosphorazidate
• CAS No.: 1417609-32-5
• Molecular Formula: C₁₀H₁₄N₃O₃P
• Molecular Weight: 255.213
• Mol file: 1417609-32-5.mol

Synonyms:

Chemical Property of butyl phenylphosphorazidate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of butyl phenylphosphorazidate

There total 3 articles about butyl phenylphosphorazidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phenol (108-95-2,27073-41-2) → butyl phenylphosphorazidate (1417609-32-5)

Guidance literature:

Multi-step reaction with 3 steps

1: trichlorophosphate; triethylamine / diethyl ether / 1 h / Inert atmosphere; Cooling with liquid nitrogen

2: triethylamine / diethyl ether / 0.5 h / Inert atmosphere; Cooling with liquid nitrogen

3: sodium azide / acetone / Inert atmosphere; Darkness

With sodium azide; triethylamine; trichlorophosphate; In diethyl ether; acetone;

DOI:10.1039/c3cc41110a

Reference yield:

O-phenyl phosphorodichloridate (770-12-7) → butyl phenylphosphorazidate (1417609-32-5)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / diethyl ether / 0.5 h / Inert atmosphere; Cooling with liquid nitrogen

2: sodium azide / acetone / Inert atmosphere; Darkness

With sodium azide; triethylamine; In diethyl ether; acetone;

DOI:10.1039/c3cc41110a

Reference yield:

Chlorophosphoric Acid Butyl Phenyl Ester (6719-82-0) → butyl phenylphosphorazidate (1417609-32-5)

Guidance literature:

With sodium azide; In acetone; Inert atmosphere; Darkness;

DOI:10.1039/c3cc41110a

upstream raw materials:

phenol

Chlorophosphoric Acid Butyl Phenyl Ester

O-phenyl phosphorodichloridate