1,4-Dimethyl-5-phenethyl-1,2,5,6-tetrahydropyridin

Base Information

Chemical Name:1,4-Dimethyl-5-phenethyl-1,2,5,6-tetrahydropyridin
CAS No.:154388-84-8
Molecular Formula:C₁₅H₂₁N
Molecular Weight:215.338
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,4-Dimethyl-5-phenethyl-1,2,5,6-tetrahydropyridin

Chemical Property:

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Technology Process of 1,4-Dimethyl-5-phenethyl-1,2,5,6-tetrahydropyridin

There total 8 articles about 1,4-Dimethyl-5-phenethyl-1,2,5,6-tetrahydropyridin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-Methyl-4-phenethyl-1,5-dichlor-2-penten

: 74-89-5
methylamine

: 154388-84-8
1,4-Dimethyl-5-phenethyl-1,2,5,6-tetrahydropyridin

Guidance literature:: With potassium iodide; In ethanol; at 60 ℃; for 20h; Yield given;
DOI:10.1002/ardp.19943270214

Reference yield:

: 5337-63-3
ethyl 2-(2-phenylethyl)acetoacetate

: 154388-84-8
1,4-Dimethyl-5-phenethyl-1,2,5,6-tetrahydropyridin

Guidance literature:: Multi-step reaction with 7 steps

1: 60 percent / p-toluenesulphonic acid / CHCl₃ / 6 h / Heating

2: 81 percent / LiAlH₄ / diethyl ether / 0.5 h / Heating

3: 71 percent / p-toluenesulphonic acid / acetone / 1.5 h / Heating

4: 1.) 80percent NaH / 1.) THF, 25 min, 2.) 3 h

5: 90 percent / LiAlH₄ / diethyl ether / 0.5 h / Heating

6: PPh₃, CCl₄ / 3 h / Heating

7: KI / ethanol / 20 h / 60 °C

With tetrachloromethane; lithium aluminium tetrahydride; sodium hydride; toluene-4-sulfonic acid; triphenylphosphine; potassium iodide; In diethyl ether; ethanol; chloroform; acetone;
DOI:10.1002/ardp.19943270214

Reference yield:

: 154388-88-2
2-Acetyl-4-phenylbutanol

: 154388-84-8
1,4-Dimethyl-5-phenethyl-1,2,5,6-tetrahydropyridin

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 80percent NaH / 1.) THF, 25 min, 2.) 3 h

2: 90 percent / LiAlH₄ / diethyl ether / 0.5 h / Heating

3: PPh₃, CCl₄ / 3 h / Heating

4: KI / ethanol / 20 h / 60 °C

With tetrachloromethane; lithium aluminium tetrahydride; sodium hydride; triphenylphosphine; potassium iodide; In diethyl ether; ethanol;
DOI:10.1002/ardp.19943270214