μ-oxobis(chlorotriphenylantimony(V))benzene solvate (1/2)

Base Information

Chemical Name:μ-oxobis(chlorotriphenylantimony(V))benzene solvate (1/2)
CAS No.:115730-70-6
Molecular Formula:C₃₆H₃₀Cl₂OSb₂
Molecular Weight:793.04
Hs Code.:

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Chemical Property of μ-oxobis(chlorotriphenylantimony(V))benzene solvate (1/2)

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Technology Process of μ-oxobis(chlorotriphenylantimony(V))benzene solvate (1/2)

There total 1 articles about μ-oxobis(chlorotriphenylantimony(V))benzene solvate (1/2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 603-36-1
triphenylantimony

: silver(I) chloride

: 106436-42-4,115730-70-6,1538-63-2
μ-oxobis(chlorotriphenylantimony(V))benzene solvate (1/2)

Guidance literature:: In acetonitrile; mixing (SbPh3 : AgCl = 3 : 1);
DOI:10.1071/C96042

Reference yield: 80.0%

: 3425-46-5
potassium selenocyanate

: 1538-63-2,115730-70-6,106436-42-4
μ-oxy-bis(triphenylantimony) dichloride

: μ-oxy-bis(triphenylantimony) bis-selenocyanate

Guidance literature:: With catalyst: 18-crown-6; In benzene; byproducts: KCl; stirring antimony complex and KSeCN in benzene at room temp. in the presence of catalytic amt. of 18-crown-6 for 4-6 h; filtration; removal of solvent in vac.; recrystn. from petroleum ether;elem. anal.;
DOI:10.1016/S0277-5387(00)84561-1