Technology Process of C14H14N4O
There total 6 articles about C14H14N4O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: acetic acid / 100 °C
2: trichlorophosphate / 70 °C
3: sodium azide; tetra(n-butyl)ammonium hydrogensulfate / dimethyl sulfoxide
4: sodium dithionite / methanol
5: 150 °C
6: palladium on activated charcoal / methanol
With
sodium azide; sodium dithionite; palladium on activated charcoal; tetra(n-butyl)ammonium hydrogensulfate; acetic acid; trichlorophosphate;
In
methanol; dimethyl sulfoxide;
DOI:10.1021/jm5002937
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium azide; tetra(n-butyl)ammonium hydrogensulfate / dimethyl sulfoxide
2: sodium dithionite / methanol
3: 150 °C
4: palladium on activated charcoal / methanol
With
sodium azide; sodium dithionite; palladium on activated charcoal; tetra(n-butyl)ammonium hydrogensulfate;
In
methanol; dimethyl sulfoxide;
DOI:10.1021/jm5002937
- Guidance literature:
-
Multi-step reaction with 5 steps
1: trichlorophosphate / 70 °C
2: sodium azide; tetra(n-butyl)ammonium hydrogensulfate / dimethyl sulfoxide
3: sodium dithionite / methanol
4: 150 °C
5: palladium on activated charcoal / methanol
With
sodium azide; sodium dithionite; palladium on activated charcoal; tetra(n-butyl)ammonium hydrogensulfate; trichlorophosphate;
In
methanol; dimethyl sulfoxide;
DOI:10.1021/jm5002937
