bis(3-[(diphenylphosphinyl)methyl]benzene-1,2-diol)silver(I) triflate N,N-dimethylformamide dichloromethane adduct (1/1/1)

Base Information

Chemical Name:bis(3-[(diphenylphosphinyl)methyl]benzene-1,2-diol)silver(I) triflate N,N-dimethylformamide dichloromethane adduct (1/1/1)
CAS No.:957665-44-0
Molecular Formula:CF₃O₃S*CH₂Cl₂*C₃H₇NO*C₃₈H₃₄AgO₄P₂
Molecular Weight:1031.6
Hs Code.:

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Chemical Property of bis(3-[(diphenylphosphinyl)methyl]benzene-1,2-diol)silver(I) triflate N,N-dimethylformamide dichloromethane adduct (1/1/1)

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Technology Process of bis(3-[(diphenylphosphinyl)methyl]benzene-1,2-diol)silver(I) triflate N,N-dimethylformamide dichloromethane adduct (1/1/1)

There total 1 articles about bis(3-[(diphenylphosphinyl)methyl]benzene-1,2-diol)silver(I) triflate N,N-dimethylformamide dichloromethane adduct (1/1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 922721-39-9
3-((diphenylphosphanyl)-methyl)-benzene-1,2-diole

: 75-09-2
dichloromethane

: 2923-28-6
silver trifluoromethanesulfonate

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 957665-44-0
bis(3-[(diphenylphosphinyl)methyl]benzene-1,2-diol)silver(I) triflate N,N-dimethylformamide dichloromethane adduct (1/1/1)

Guidance literature:: In tetrahydrofuran; (Ar); Ag salt added to a soln. of ligand, DMF added, stirred for 1 h; evapd. (vac.), dissolved in CH2Cl2, Et2O added, crystd. at -28°C;elem. anal.;
DOI:10.1039/b708252e