N-[(1R,2R)-2-azidocyclohexyl]-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-[(1R,2R)-2-azidocyclohexyl]-4-methylbenzenesulfonamide
CAS No.:339312-77-5
Molecular Formula:C₁₃H₁₈N₄O₂S
Molecular Weight:294.378
Hs Code.:
DSSTox Substance ID:DTXSID601199705
Nikkaji Number:J1.280.360E

Synonyms:DTXSID601199705;339312-77-5;N-[(1R,2R)-2-azidocyclohexyl]-4-methylbenzenesulfonamide

Suppliers and Price of N-[(1R,2R)-2-azidocyclohexyl]-4-methylbenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of N-[(1R,2R)-2-azidocyclohexyl]-4-methylbenzenesulfonamide

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:294.11504700
Heavy Atom Count:20
Complexity:459

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NC2CCCCC2N=[N+]=[N-]
Isomeric SMILES:CC1=CC=C(C=C1)S(=O)(=O)N[C@@H]2CCCC[C@H]2N=[N+]=[N-]

Technology Process of N-[(1R,2R)-2-azidocyclohexyl]-4-methylbenzenesulfonamide

There total 3 articles about N-[(1R,2R)-2-azidocyclohexyl]-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 127-65-1
chloroamine-T

: 339312-77-5
N-(2-azidocyclohexyl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: K₂OsO₂(OH)4 / 1,4-bis(dihydroquininyl)phthalazine / acetonitrile; H₂O / 6 h / Ambient temperature

2: 1.) SO₂Cl₂, Et₃N, 2.) NaH / 1.) EtOAc

3: NaN₃

With sodium azide; sulfuryl dichloride; potassium dioxotetrahydroxoosmate(VI); sodium hydride; triethylamine; (3a,9R,3'''a,4'"b,9'"R)-9,9'-[1,4-phthalazinediylbis(oxy)]bis[6'-(methyloxy)-10,11-dihydrocinchonan]; In water; acetonitrile;

Reference yield:

: (3aR,7aS)-3-(Toluene-4-sulfonyl)-hexahydro-benzo[1,2,3]oxathiazole 2,2-dioxide

: 339312-77-5
N-(2-azidocyclohexyl)-4-methyl-benzenesulfonamide

Guidance literature:: With sodium azide;

Reference yield:

: 176298-50-3
(1S,2R)-N-(p-toluenesulfonyl)-2-amino-1-hydroxycyclohexane

: 339312-77-5
N-(2-azidocyclohexyl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) SO₂Cl₂, Et₃N, 2.) NaH / 1.) EtOAc

2: NaN₃

With sodium azide; sulfuryl dichloride; sodium hydride; triethylamine;