C₂₆H₂₈N₄O₂

Base Information

• Chemical Name: C₂₆H₂₈N₄O₂
• CAS No.: 1366232-70-3
• Molecular Formula: C₂₆H₂₈N₄O₂
• Molecular Weight: 428.534
• Mol file: 1366232-70-3.mol

Synonyms:

Chemical Property of C₂₆H₂₈N₄O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₂₈N₄O₂

There total 5 articles about C₂₆H₂₈N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-Dinitrofluorobenzene (70-34-8,65727-75-5) → C26H28N4O2 (1366232-70-3)

Guidance literature:

Multi-step reaction with 4 steps

1: caesium carbonate / tetrahydrofuran

2: hydrogen; palladium on activated charcoal / ethyl acetate

3: hydrogenchloride / water / 90 °C

4: sodium tris(acetoxy)borohydride / dichloromethane

With hydrogenchloride; palladium on activated charcoal; hydrogen; sodium tris(acetoxy)borohydride; caesium carbonate; In tetrahydrofuran; dichloromethane; water; ethyl acetate;

DOI:10.1016/j.bmcl.2012.11.095

Reference yield:

N-(4-methoxyphenyl)-2,4-dinitrobenzenamine (967-35-1) → C26H28N4O2 (1366232-70-3)

Guidance literature:

Multi-step reaction with 3 steps

1: hydrogen; palladium on activated charcoal / ethyl acetate

2: hydrogenchloride / water / 90 °C

3: sodium tris(acetoxy)borohydride / dichloromethane

With hydrogenchloride; palladium on activated charcoal; hydrogen; sodium tris(acetoxy)borohydride; In dichloromethane; water; ethyl acetate;

DOI:10.1016/j.bmcl.2012.11.095

Reference yield:

4-methoxy-aniline (104-94-9) → C26H28N4O2 (1366232-70-3)

Guidance literature:

Multi-step reaction with 4 steps

1: caesium carbonate / tetrahydrofuran

2: hydrogen; palladium on activated charcoal / ethyl acetate

3: hydrogenchloride / water / 90 °C

4: sodium tris(acetoxy)borohydride / dichloromethane

With hydrogenchloride; palladium on activated charcoal; hydrogen; sodium tris(acetoxy)borohydride; caesium carbonate; In tetrahydrofuran; dichloromethane; water; ethyl acetate;

DOI:10.1016/j.bmcl.2012.11.095

upstream raw materials:

4-(morpholin-4-ylmethyl)benzaldehyde

1-(4-methoxyphenyl)-5-aminobenzimidazole

2,4-Dinitrofluorobenzene

N-(4-methoxyphenyl)-2,4-dinitrobenzenamine