mesylate derivative

Base Information

• Chemical Name: mesylate derivative
• CAS No.: 57590-62-2
• Molecular Formula: C₁₀H₁₆N₂O₂S
• Molecular Weight: 228.315
• Mol file: 57590-62-2.mol

Synonyms:

Chemical Property of mesylate derivative

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of mesylate derivative

There total 1 articles about mesylate derivative which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2-hydroxyethyl)-N-methylaminobenzene (93-90-3) + methanesulfonyl chloride (124-63-0) → mesylate derivative (57590-62-2)

Guidance literature:

With triethylamine; In dichloromethane; at 4 - 20 ℃; for 1h; Inert atmosphere;

DOI:10.1002/chem.201203427

Reference yield:

mesylate derivative (57590-62-2) → N-(2-azidoethyl)-N-methylaniline (1249429-26-2)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 40 ℃;

DOI:10.1002/chem.201203427

Reference yield:

mesylate derivative (57590-62-2) → C31H32N9(1+)*C2F3O2(1-) (1432151-27-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium azide / N,N-dimethyl-formamide / 40 °C

2.1: nitrosonium tetrafluoroborate / acetonitrile / 0.25 h / 0 °C

2.2: 1 h / 0 °C

With sodium azide; nitrosonium tetrafluoroborate; In N,N-dimethyl-formamide; acetonitrile;

DOI:10.1002/chem.201203427

upstream raw materials:

N-(2-hydroxyethyl)-N-methylaminobenzene

methanesulfonyl chloride

Downstream raw materials:

C₃₁H₃₂N₉⁽¹⁺⁾*C₂F₃O₂^(1-)

C₄₁H₄₀N₉O₂⁽¹⁺⁾*C₂F₃O₂^(1-)

C₃₉H₄₁N₁₁O₇S*C₂HF₃O₂

N-(2-azidoethyl)-N-methylaniline