N-methyl-2-(2-hydroxy-5-methoxy-4-(pentylthio)phenyl)-3-methylbutylamine

Base Information

Chemical Name:N-methyl-2-(2-hydroxy-5-methoxy-4-(pentylthio)phenyl)-3-methylbutylamine
CAS No.:129658-15-7
Molecular Formula:C₁₈H₃₁NO₂S
Molecular Weight:325.516
Hs Code.:

Synonyms:

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Chemical Property of N-methyl-2-(2-hydroxy-5-methoxy-4-(pentylthio)phenyl)-3-methylbutylamine

Chemical Property:

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Technology Process of N-methyl-2-(2-hydroxy-5-methoxy-4-(pentylthio)phenyl)-3-methylbutylamine

There total 7 articles about N-methyl-2-(2-hydroxy-5-methoxy-4-(pentylthio)phenyl)-3-methylbutylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-53-2
1-Bromopentane

: 129658-15-7
N-methyl-2-(2-hydroxy-5-methoxy-4-(pentylthio)phenyl)-3-methylbutylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / EtONa / ethanol / 5 h / Heating

2: 1.) HCl / 1.) dioxane, water, 65 deg C, 10 min, 2.) 60 to 65 deg C, 30 min

3: 86 percent / dimethylformamide / 5.5 h / 40 - 95 °C

4: 1.) NaH / 1.) DMF, from 40 to 50 deg C, 30 min, 2.) 60 deg C, 6 h

5: LiAlH₄, AlCl₃ / diethyl ether / 6 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; sodium ethanolate; sodium hydride; In diethyl ether; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 1483-27-8
2,5-dimethoxythiophenol

: 129658-15-7
N-methyl-2-(2-hydroxy-5-methoxy-4-(pentylthio)phenyl)-3-methylbutylamine

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / EtONa / ethanol / 5 h / Heating

2: 1.) HCl / 1.) dioxane, water, 65 deg C, 10 min, 2.) 60 to 65 deg C, 30 min

3: 86 percent / dimethylformamide / 5.5 h / 40 - 95 °C

4: 1.) NaH / 1.) DMF, from 40 to 50 deg C, 30 min, 2.) 60 deg C, 6 h

5: LiAlH₄, AlCl₃ / diethyl ether / 6 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; sodium ethanolate; sodium hydride; In diethyl ether; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 129658-04-4
1,4-dimethoxy-2-(pentylthio)benzene

: 129658-15-7
N-methyl-2-(2-hydroxy-5-methoxy-4-(pentylthio)phenyl)-3-methylbutylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) HCl / 1.) dioxane, water, 65 deg C, 10 min, 2.) 60 to 65 deg C, 30 min

2: 86 percent / dimethylformamide / 5.5 h / 40 - 95 °C

3: 1.) NaH / 1.) DMF, from 40 to 50 deg C, 30 min, 2.) 60 deg C, 6 h

4: LiAlH₄, AlCl₃ / diethyl ether / 6 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; aluminium trichloride; sodium hydride; In diethyl ether; N,N-dimethyl-formamide;